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DUAN Hong-ying, LIANG Guo-li, MIAO Jian-min. Determination of 37 Major, Minor and Trace Elements in Ancient Ceramics by Wavelength Dispersive X-ray Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2011, 30(3): 337-342.
Citation: DUAN Hong-ying, LIANG Guo-li, MIAO Jian-min. Determination of 37 Major, Minor and Trace Elements in Ancient Ceramics by Wavelength Dispersive X-ray Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2011, 30(3): 337-342.
shu

Determination of 37 Major, Minor and Trace Elements in Ancient Ceramics by Wavelength Dispersive X-ray Fluorescence Spectrometry

  • 1.

    Key Scientific Research Base of Ancient Ceramics, State Administration of Cultural Heritage(The Palace Museum), Beijing 100009, China

  • 2.

    Conservation Technology Department of the Palace Museum, Beijing 100009, China

  • 3.

    Key Scientific Research Base of Ancient Ceramics, State Administration of Cultural Heritage(The Palace Museum), Beijing 100009, China

  • 4.

    National Research Center for Geoanalysis, Beijing 100037, China

  • 5.

    Key Scientific Research Base of Ancient Ceramics, State Administration of Cultural Heritage(The Palace Museum), Beijing 100009, China

  • 6.

    Conservation Technology Department of the Palace Museum, Beijing 100009, China

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  • Received Date: August 24, 2010
  • Revised Date: December 19, 2010
    Abstract
  • A method for the determination of Na2O, MgO, Al2O3, SiO2, P2O5, K2O, CaO, Sc, TiO2, V2O5, Cr2O3, MnO, Fe2O3, CoO, NiO, CuO, ZnO, Ga, As, Br, Rb, Sr, Y, Zr, Nb, Sn, Sb, Cs, BaO, La, Ce, Nd, Sm, Hf, PbO, Bi and Th in pressed power pellets of ancient ceramics body and glaze by X ray fluorescence spectrometry was reported in this paper. The matrix effect was corrected by experience coefficients, Compton scattering and background as internal standard for trace elements determination. The method has been verified by analyzing the national standard Reference Materials of topsoil and stream sediment and the analytical results were in agreement with the certified values, and RSD (n=11) of most elements (except four elements) are less than 10%, indicating that our method has a high accuracy and can greatly satisfy ancient ceramics research work. The method has been applied to the determination of seven ancient ceramics samples. The obtained results were consistent with the results of other analysis methods.
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    • References (17)
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