• Core Journal of China
  • DOAJ
  • Scopus
  • Chinese Scientific and Technical Papers and Citations (CSTPC)
  • Chinese Science Citation Database (CSCD)
SHEN Dong-xu, LIAN Hong-zhen, DING Tao, SHEN Chong-yu. A Review on the Analysis of Photoinitiator Residues[J]. Rock and Mineral Analysis, 2011, 30(1): 104-109.
Citation: SHEN Dong-xu, LIAN Hong-zhen, DING Tao, SHEN Chong-yu. A Review on the Analysis of Photoinitiator Residues[J]. Rock and Mineral Analysis, 2011, 30(1): 104-109.

A Review on the Analysis of Photoinitiator Residues

More Information
  • Received Date: June 06, 2010
  • The analysis of photoinitiator residues was lately developed. The advanced high-sensitive analytical techniques have been usually applied to the analysis of photoinitiator residues because of their lower concentration level. In this paper, the definition of photoinitiators including Benzophenone, ITX, Irgacure 184, Irgacure 907, Irgacure 369, TPO, EHA was introduced as well as their types, sources and harmfulness. The detection technologies of photoinitiator residues, such as gas chromatography-mass spectrometry (GC-MS), paper chromatography-mass spectrometry and liquid chromatography-mass spectrometry were summarized. Because of the technical limit of gas chromatography, liquid chromatography-mass spectrometry was more commonly applied to the detection of photoinitiator residues. The different procedures of sample pretreatment, such as liquid-liquid extraction, accelerated solvent extraction (ASE), solid phase extraction (SPE), etc. were compared. Comparing with other pretreatment technologies, solid phase extraction is more mature and suitable for high-throughput analysis of photoinitiator residues. The detection of photoinitiator residues and the simultaneous detection of pesticide residues and veterinary drug residues are the direction of future development.
  • The European Food Safety Authority.Opinion of the scientific panel of food additives, flavourings, processing, aids and materials in contact with food on a request from the commission related to 2-isopropyl thioxanthone (ITX) and 2-ethylhexyl-4-dimethylamino-benzoate (EHDAB) in food contact materials .2005.

    The European Food Safety Authority.Opinion of the scientific panel of food additives, flavourings, processing, aids and materials in contact with food on a request from the commission related to 2-isopropyl thioxanthone (ITX) and 2-ethylhexyl-4-dimethylamino-benzoate (EHDAB) in food contact materials .2005.
    魏杰,金养智.光固化涂料 [M].北京:化学工业出版社, 2005: 68-70.
    Rhodes M C, Bucher J R, Peckham J C, Kissling G E, Hejtmancik M R, Chhabra R S. Carcinogenesis studies of benzophenone in rats and mice [J].Food and Chemical Toxicology,2007,45(5): 843-851.

    Rhodes M C, Bucher J R, Peckham J C, Kissling G E, Hejtmancik M R, Chhabra R S. Carcinogenesis studies of benzophenone in rats and mice [J].Food and Chemical Toxicology,2007,45(5): 843-851.
    Hsieh M H, Granthama E C, Liu B, Macapagal R, Willingham E, Baskin L S. In utero exposure to benzophenone-2 causes hypospadias through an estrogen receptor dependent mechanism [J].The Journal of Urology,2007,178(4):1637-1742.

    Hsieh M H, Granthama E C, Liu B, Macapagal R, Willingham E, Baskin L S. In utero exposure to benzophenone-2 causes hypospadias through an estrogen receptor dependent mechanism [J].The Journal of Urology,2007,178(4):1637-1742.
    Cook N, Freeman S. Report of 19 cases of photoallergic contact dermatitis to sunscreens seen at the skin and cancer foundation [J].Australasian Journal of Dermatology,2001,42:257-259.

    Cook N, Freeman S. Report of 19 cases of photoallergic contact dermatitis to sunscreens seen at the skin and cancer foundation [J].Australasian Journal of Dermatology,2001,42:257-259.
    Momo F, Fabris S, Stevanato R. Interaction of isopro-pylthioxanthone with phospholipid liposomes [J].Biophy-sical Chemistry,2007,127(1-2):36-40.

    Momo F, Fabris S, Stevanato R. Interaction of isopro-pylthioxanthone with phospholipid liposomes [J].Biophy-sical Chemistry,2007,127(1-2):36-40.
    Peijnenburg A, Riethof-Poortman J, Baykus H, Portier L, Bovee T, Hoogenboom R. AhR-agonistic, anti-androgenic, and anti-estrogenic potencies of 2-isopropylthioxanthone (ITX) as determined by in vitro bioassays and gene expression profiling [J].Toxicology in Vitro,2010,24(6):1619-1628.

    Peijnenburg A, Riethof-Poortman J, Baykus H, Portier L, Bovee T, Hoogenboom R. AhR-agonistic, anti-androgenic, and anti-estrogenic potencies of 2-isopropylthioxanthone (ITX) as determined by in vitro bioassays and gene expression profiling [J].Toxicology in Vitro,2010,24(6):1619-1628.
    Allegrone G, Tamaro I, Spinardi S, Grosa G. Development and validation of a solid-phase extraction and gas chromatography tandem mass spectrometry method for the determination of isopropyl-9H-thioxanthen-9-one in carton packaged milk [J].Journal of Chromatography A,2008,1214(1-2):128-133.

    Allegrone G, Tamaro I, Spinardi S, Grosa G. Development and validation of a solid-phase extraction and gas chromatography tandem mass spectrometry method for the determination of isopropyl-9H-thioxanthen-9-one in carton packaged milk [J].Journal of Chromatography A,2008,1214(1-2):128-133.
    邓晓军,郭德华,李波,朱坚,殷平.气相色谱-质谱法测定乳制品中光引发剂异丙基硫杂蒽酮的残留量[J].分析化学,2007,25(1):39-42.
    Morlock G, Schwack W. Determination of isopropylthio-xanthone (ITX) in milk, yoghurt and fat by HPTLC-FLD, HPTLC-ESI/MS and HPTLC-DART/MS [J].Analytical and Bioanalytical Chemistry,2006,385(3):586-595.

    Morlock G, Schwack W. Determination of isopropylthio-xanthone (ITX) in milk, yoghurt and fat by HPTLC-FLD, HPTLC-ESI/MS and HPTLC-DART/MS [J].Analytical and Bioanalytical Chemistry,2006,385(3):586-595.
    Gallart-Ayala H, Moyano E, Galceran M T. Liquid chromatography/tandem mass spectrometry (highly sele-ctive selected reaction monitoring) for the analysis of isopropylthioxanthone in packaged food [J].Journal of Chromatography A, 2008, 1208(1-2): 182-188.

    Gallart-Ayala H, Moyano E, Galceran M T. Liquid chromatography/tandem mass spectrometry (highly sele-ctive selected reaction monitoring) for the analysis of isopropylthioxanthone in packaged food [J].Journal of Chromatography A, 2008, 1208(1-2): 182-188.
    Bagnati R, Bianchi G, Marangon E, Zuccato E, Fanelli R, Davoli E. Direct analysis of isopropylthioxanthone (ITX) in milk by high-performance liquid chromatography/tandem mass spectrometry [J].Rapid Communication in Mass Spectrometry, 2007, 21(13): 1998-2002.

    Bagnati R, Bianchi G, Marangon E, Zuccato E, Fanelli R, Davoli E. Direct analysis of isopropylthioxanthone (ITX) in milk by high-performance liquid chromatography/tandem mass spectrometry [J].Rapid Communication in Mass Spectrometry, 2007, 21(13): 1998-2002.
    Sun C L, Chan S H, Lu D, Lee H M W, Bloodworth B C. Determination of isopropyl-9H-thioxanthen-9-one in pack-aged beverages by solid-phase extraction clean-up and liquid chromatography with tandem mass spectrometry detection [J].Journal of Chromatography A,2007,1143(1-2):162-167.

    Sun C L, Chan S H, Lu D, Lee H M W, Bloodworth B C. Determination of isopropyl-9H-thioxanthen-9-one in pack-aged beverages by solid-phase extraction clean-up and liquid chromatography with tandem mass spectrometry detection [J].Journal of Chromatography A,2007,1143(1-2):162-167.
    Benetti C, Angeletti R, Binato G, Biancardi A, Biancotto G . A packaging contaminant: Isopropylthioxanthone (ITX) in dairy products [J].Analytica Chimica Acta,2008,617(1-2):132-138.

    Benetti C, Angeletti R, Binato G, Biancardi A, Biancotto G . A packaging contaminant: Isopropylthioxanthone (ITX) in dairy products [J].Analytica Chimica Acta,2008,617(1-2):132-138.
    Sagratini G, Manes J, Giardina D, Pico Y. Determination of isopropyl thioxanthone (ITX) in fruit juices by pressurized liquid extraction and liquid chromatography-mass spectrometry [J].Journal of Agricultural and Food Chemistry,2006,54(20):7947-7952.

    Sagratini G, Manes J, Giardina D, Pico Y. Determination of isopropyl thioxanthone (ITX) in fruit juices by pressurized liquid extraction and liquid chromatography-mass spectrometry [J].Journal of Agricultural and Food Chemistry,2006,54(20):7947-7952.
    Gil-Vergara A, Blasco C, Pico Y.Determination of 2-isopropylthioxanthone and 2-ethylhexyl-4-dimethylamino-benzoate in milk: Comparison of gas and liquid chromatography with mass spectrometry [J].Analytical and Bioanalytical Chemistry,2007,389(2):605-617.

    Gil-Vergara A, Blasco C, Pico Y.Determination of 2-isopropylthioxanthone and 2-ethylhexyl-4-dimethylamino-benzoate in milk: Comparison of gas and liquid chromatography with mass spectrometry [J].Analytical and Bioanalytical Chemistry,2007,389(2):605-617.
    Sanches-Silva A, Pastorelli S, Cruz J M, Simoneau C, Castanheira I, Paseiro-Losada P.Development of a method to study the migration of six photoinitiators into powdered milk [J].Journal of Agricultural and Food Chemistry,2008,56(8): 2722-2726.

    Sanches-Silva A, Pastorelli S, Cruz J M, Simoneau C, Castanheira I, Paseiro-Losada P.Development of a method to study the migration of six photoinitiators into powdered milk [J].Journal of Agricultural and Food Chemistry,2008,56(8): 2722-2726.
    Sanches-Silva A, Pastorelli S, Cruz J M, Simoneau C, Paseiro-Losada P. Development of a multi-method for the determination of photoinitiators in beverage packaging [J].Journal of Food Science,2008,73(2):C92-C99.

    Sanches-Silva A, Pastorelli S, Cruz J M, Simoneau C, Paseiro-Losada P. Development of a multi-method for the determination of photoinitiators in beverage packaging [J].Journal of Food Science,2008,73(2):C92-C99.
    Sagratini G, Caprioli G, Cristalli G, Giardina D, Ricciutelli M, Volpini R, Zuo Y T, Vittori S. Determination of ink photoinitiators in packaged beverages by gas chromato-graphy-mass spectrometry and liquid chromatography-mass spectrometry [J].Journal of Chromatography A,2008,1194(2):213-220.

    Sagratini G, Caprioli G, Cristalli G, Giardina D, Ricciutelli M, Volpini R, Zuo Y T, Vittori S. Determination of ink photoinitiators in packaged beverages by gas chromato-graphy-mass spectrometry and liquid chromatography-mass spectrometry [J].Journal of Chromatography A,2008,1194(2):213-220.
    Shen D X, Lian H Z, Ding T, Xu J Z, Shen C Y. Determination of low-level ink photoinitiator residues in packaged milk by solid-phase extraction and LC-ESI/MS/MS using triple-quadrupole mass analyzer [J].Analytical and Bioanalytical Chemistry,2009,395(7): 2359-2370.

    Shen D X, Lian H Z, Ding T, Xu J Z, Shen C Y. Determination of low-level ink photoinitiator residues in packaged milk by solid-phase extraction and LC-ESI/MS/MS using triple-quadrupole mass analyzer [J].Analytical and Bioanalytical Chemistry,2009,395(7): 2359-2370.
    李攻科,胡玉玲, 阮贵华.样品前处理仪器与装置 [M].北京:化学工业出版社, 2007: 4-10.
    D' Archivio A A, Fanelli M, Mazzeo P, Ruggieri F. Comparison of different sorbents for multi-residue solid-phase extraction of 16 pesticides from groundwater coupled with high-performance liquid chromatography [J].Talanta,2007,71(1):25-30.

    D' Archivio A A, Fanelli M, Mazzeo P, Ruggieri F. Comparison of different sorbents for multi-residue solid-phase extraction of 16 pesticides from groundwater coupled with high-performance liquid chromatography [J].Talanta,2007,71(1):25-30.
    Rodil R, Quintana J B, Lopez-Mahia P, Muniategui-Lorenzo S, Prada-Rodriguez D. Multi-residue analytical method for the determination of emerging pollutants in water by solid-phase extraction and liquid chromatography-tandem mass spectrometry [J].Journal of Chromatography A,2009,1216(14):2958-2969.

    Rodil R, Quintana J B, Lopez-Mahia P, Muniategui-Lorenzo S, Prada-Rodriguez D. Multi-residue analytical method for the determination of emerging pollutants in water by solid-phase extraction and liquid chromatography-tandem mass spectrometry [J].Journal of Chromatography A,2009,1216(14):2958-2969.
  • Related Articles

    [1]LI Ying-chun, ZHANG Lei, SHANG Wen-yu. Determination of Selenium, Major and Minor Elements in Selenium-rich Soil Samples by X-ray Fluorescence Spectrometry with Powder Pellet Preparation[J]. Rock and Mineral Analysis, 2022, 41(1): 145-152. DOI: 10.15898/j.cnki.11-2131/td.202007090102
    [2]Wei ZHOU, Meng ZENG, Jian WANG, Lei ZHANG, Ying-chun LI. Determination of Major and Rare Earth Elements in Rare Earth Ores by X-ray Fluorescence Spectrometry with Fusion Sample Preparation[J]. Rock and Mineral Analysis, 2018, 37(3): 298-305. DOI: 10.15898/j.cnki.11-2131/td.201706280113
    [3]Jing CHEN, Zhi-jun GAO, Chong-ke CHEN, Yan-xia LIU, Ming-wei ZHANG. Application Skills on Determination of Geological Sample by X-ray Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2015, 34(1): 91-98. DOI: 10.15898/j.cnki.11-2131/td.2015.01.012
    [4]LUO Xue-hui, SU Jian-zhi, LU Qing, YANG Li-qin, WANG Lan. Fused Pellet-Determination of 16 Elements in Copper Ores by X-ray Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2014, 33(2): 230-235.
    [5]MA Tian-fang, LI Xiao-li, CHEN Yong-jun, DENG Zhen-pin, LI Guo-hui. Interchangeable Analysis of Method on the X-ray Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2011, 30(4): 486-490.
    [6]Simultaneous Determination of Major, Minor and Trace Components in Limestone Samples by X-ray Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2008, 27(2): 149-150.
    [7]Determination of Silicon and Iron in Zn-Al-Si Alloy by X-ray Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2008, 27(1): 77-78.
    [8]X-ray Fluorescence Spectrometric Analysis of Major Components in Bauxite Samples[J]. Rock and Mineral Analysis, 2008, 27(1): 71-73.
    [9]Discussion on the Detection Limit in X-Ray Fluorescence Spectrometric Analysis[J]. Rock and Mineral Analysis, 2003, (4): 291-296.
    [10]Standardization of X-Ray Fluorescence Spectrometric Analysis[J]. Rock and Mineral Analysis, 2002, (1): 42-48.

Catalog

    Article views (1880) PDF downloads (1836) Cited by()

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return