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LI Yi, DONG Jian-fang, ZHANG Yu. Gas Chromatography-Mass Spectrometric Determination of Volatile Organic Compounds in Groundwater with Purge and Trap Sampling[J]. Rock and Mineral Analysis, 2010, 29(5): 513-517.
Citation: LI Yi, DONG Jian-fang, ZHANG Yu. Gas Chromatography-Mass Spectrometric Determination of Volatile Organic Compounds in Groundwater with Purge and Trap Sampling[J]. Rock and Mineral Analysis, 2010, 29(5): 513-517.
shu

Gas Chromatography-Mass Spectrometric Determination of Volatile Organic Compounds in Groundwater with Purge and Trap Sampling

  • 1.

    Hebei Institute of Environmental Geological Exploration, Shijiazhuang 050021, China

  • 2.

    Hebei Institute of Environmental Geological Exploration, Shijiazhuang 050021, China

  • 3.

    College of Geoscience and Surveying Engineering, China University of Mining & Technology, Beijing 100083, China

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  • Received Date: January 17, 2010
  • Revised Date: June 02, 2010
    Abstract
  • A method was developed for simultaneous detection of more than 20 volatile organic compounds (VOCs) including halogenated hydrocarbons, benzene series compounds, aromatic hydrocarbons and chlorinated benzenes in groundwater by gas chromatography-mass spectrometry with purge and trap sampling. The experimental conditions of purge and trap sampling and gas chromatography-mass spectrometric determination were optimized. The detection limits of the method for the volatile organic compounds were 0.03~0.28 μg/L. The recovery rates were 88.8%~111.0% with precision of 2.21%~5.31%RSD (n=7). The results show that the method is sensitive, accurate and suitable for the determination of trace VOCs in groundwater.
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    • References (19)
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