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LAI Yong-zhong. Determination of Pyridine in Drinking Source Water by Head Space Sampling-Solid Phase Microextraction[J]. Rock and Mineral Analysis, 2011, 30(5): 596-600.
Citation: LAI Yong-zhong. Determination of Pyridine in Drinking Source Water by Head Space Sampling-Solid Phase Microextraction[J]. Rock and Mineral Analysis, 2011, 30(5): 596-600.
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Determination of Pyridine in Drinking Source Water by Head Space Sampling-Solid Phase Microextraction

  • Shantou Enviromental Monitoring Station, Shantou 515041, China

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  • Received Date: March 04, 2011
  • Revised Date: May 12, 2011
    Abstract
  • Pyridine in 15 mL aqueous sample was micro-extracted by using a head space sampling-solid phase microextration system of 75 μm CarboxenTM-Polydimethylsiloxane (CAR-PDMS) fiber. The extractants were measured by Gas Chromatography-Mass Spectrometry (GC-MS) with selected ion monitoring (SIM) mode and internal standard quantitative method. Under the optimum conditions of an extraction temperature of 58.0℃ for 40 min, detection limit, correlation coefficient and linear range were 1.5 μg/L, 0.9994 and 2.5-50.0 μg/L, respectively. The obtained average values of recovery were 75.6%-81.3% (n=6) and the relative standard deviation was 9.60%-12.61% for drinking water samples and pure water with interior spike. Head space sampling-solid phase microextraction (HS-SPME), an organic solvent-free pre-processing method for water sample, can protect SPME coatings, especially for dirty samples. An MS detector has advantages in qualitative analysis and avoids the fake positive signal effect. Head space-solid phase microextraction is a convenient and sensitive method, which is capable of analyzing pyridine in drinking water.
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