Research Progress <em>in situ</em> Hf Isotopic Analysis of Oxide-type U-bearing Accessory Minerals

CUI Yurong; XIAO Zhibin; TU Jiarun; ZHOU Hongying; LI Guozhan

doi:10.15898/j.cnki.11-2131/td.202205180104

Rock and Mineral Analysis > 2022 > 41(5): 691-703. > DOI: 10.15898/j.cnki.11-2131/td.202205180104

CUI Yurong, XIAO Zhibin, TU Jiarun, ZHOU Hongying, LI Guozhan. Research Progress in situ Hf Isotopic Analysis of Oxide-type U-bearing Accessory Minerals[J]. Rock and Mineral Analysis, 2022, 41(5): 691-703. DOI: 10.15898/j.cnki.11-2131/td.202205180104

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Research Progress in situ Hf Isotopic Analysis of Oxide-type U-bearing Accessory Minerals

CUI Yurong^{1, 2,},
XIAO Zhibin^{1, 2},
TU Jiarun^{1, 2},
ZHOU Hongying^{1, 2},
LI Guozhan^{1, 2}

1.
Tianjin Center, China Geological Survey, Tianjin 300170, China
2.
North China Center for Geoscience Innovation, Tianjin 300170, China

More Information

Received Date: May 17, 2022
Revised Date: July 11, 2022
Accepted Date: August 19, 2022
Available Online: November 10, 2022

Abstract

HIGHLIGHTS
(1) Developing in situ Hf isotopic determination method for the oxide-type U-bearing accessory minerals has important scientific significance.

(2) The correction strategies for isobaric interference on oxide-type U-bearing accessory minerals, such as rutile, cassiterite and columbite, were discussed.

(3) Three schemes for developing matrix-matched reference materials were reviewed.

ABSTRACT

BACKGROUND
In recent years, the in situ Hf isotopic determination method of zircon has been widely used in isotopic geochemistry, and has become an important method to explore the genesis of rocks, the source of ore-forming materials and the evolution of crust and mantle. However, for some rocks, the lack of zircon seriously hinders the restriction of formation and evolution. The development of Hf isotopic determination methods for oxide-type U-bearing accessory minerals, such as rutile, cassiterite and columbite is urgently needed.
OBJECTIVES
In order to accelerate the studies of in situ Hf isotopic determination of oxide-type U-bearing minerals and their application to the geological research.
METHODS
In situ Hf isotopic analysis of oxide-type U-bearing accessory minerals was reviewed with NEPTUNE multiple-collector inductively coupled plasma-mass spectrometry (MC-ICPMS) and a 193nm excimer laser ablation system.
RESULTS
Combined with relevant research work in recent years, the development history of Lu-Hf isotope analysis technology for accessory minerals was briefly described, and the latest progress and existing problems in in-situ Hf isotope determination methods for oxide-type uranium-bearing minerals such as rutile, cassiterite and niobite were systematically reviewed. The current technical difficulties such as the correction strategy for isobaric interference, the lack of quality control standard samples, the lower Hf content, and the improvement of analytical sensitivity were discussed in detail.
CONCLUSIONS
The low Hf content of oxide-type U-bearing accessory minerals requires a larger spot diameter. The femtosecond laser has the characteristics of fine and uniform grain size of the ablation samples. The combination of femtosecond laser and MC-ICPMS (fs-LA-MC-ICPMS) can reduce the spot diameter and improve the spatial resolution, which is the development direction of in situ Hf isotope analysis of oxide-type U-bearing accessory minerals in the future.
- hafnium isotope,
- LA-MC-ICPMS,
- rutile,
- cassiterite,
- columbite,
- correction strategies for isobars interference

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References (78)

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Research Progress in situ Hf Isotopic Analysis of Oxide-type U-bearing Accessory Minerals