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FAN Chen-zi, HU Ming-yue, ZHAO Ling-hao, SUN Dong-yang, ZHAN Xiu-chun. Advances in in situ Microanalysis of U-Pb Zircon Geochronology Using Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry[J]. Rock and Mineral Analysis, 2012, 31(1): 29-46.
Citation: FAN Chen-zi, HU Ming-yue, ZHAO Ling-hao, SUN Dong-yang, ZHAN Xiu-chun. Advances in in situ Microanalysis of U-Pb Zircon Geochronology Using Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry[J]. Rock and Mineral Analysis, 2012, 31(1): 29-46.

Advances in in situ Microanalysis of U-Pb Zircon Geochronology Using Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry

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  • Received Date: November 23, 2011
  • Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry (LA-ICP-MS) analysis is one of the most popular methods for isotope geochronology of zircon. This technique was applied to accurately and rapidly demonstrate the age heterogeneities within a single zircon crystal. In this review the main stages of the evolution of this in situ microanalysis technique, including laser ablation system, ICP-MS, U-Pb dating methodology of zircon and applications are summarized. The influences from the laser device, ablation cell, laser ablation parameters (laser wavelength, laser pulse duration, ambient gas and crater size), quadrupole and magnetic sector ICP-MS on the precision and accuracy of U-Pb dating data are discussed. The quantitative calibration with natural zircon age standards and other standards, single U/Pb ratios calculation, correction for common Pb and simultaneous determinations of U-Pb age and trace element compositions are also introduced in this paper. At present, there are numerous zircon U-Pb geochronlogical applications for tracing sedimentary provenance studies and dating magmatic events by LA-ICP-MS.
  • Lee J K W, Williams I S, Ellis D. Pb, U and Th diffusion in natural zircon [J].Nature,1997, 390:159-163.

    Lee J K W, Williams I S, Ellis D. Pb, U and Th diffusion in natural zircon [J].Nature,1997, 390:159-163.
    Cherniak D J, Watson E B. Pb diffusion in zircon [J].Chemical Geology,2000, 172:5-24.

    Cherniak D J, Watson E B. Pb diffusion in zircon [J].Chemical Geology,2000, 172:5-24.
    吴元保,郑永飞. 锆石成因矿物学研究及其对U-Pb年龄解释的制约 [J].科学通报,2004, 49(16):1589-1604.
    李惠民,李怀坤,陈志宏,相振群,陆松年,周红英,宋彪. 基性岩斜锆石U-Pb同位素定年3种方法之比较 [J].地质通报,2007, 26(2):128-135.
    Liu Y, Li X H, Tang G Q, Yin Q Z. Precise U-Pb zircon dating at a scale of <5 micro by the CAMERA 1280 SIMS using a Gaussian illumination probe [J].Journal of Analytical Atomic Spectrometry,2011,26:845-851.

    Liu Y, Li X H, Tang G Q, Yin Q Z. Precise U-Pb zircon dating at a scale of <5 micro by the CAMERA 1280 SIMS using a Gaussian illumination probe [J].Journal of Analytical Atomic Spectrometry,2011,26:845-851.
    Gray A L. Solid sample introduction by laser ablation for inductively coupled plasma source mass spectrometry [J].Analyst,1985,110:551-556.

    Gray A L. Solid sample introduction by laser ablation for inductively coupled plasma source mass spectrometry [J].Analyst,1985,110:551-556.
    Arevalo R Jr, Bellucci J, McDonough W F. GGR bien-nial review: Advances in laser ablation and solution ICP-MS from 2008 to 2009 with particular emphasis on sensitivity enhancements, mitigation of fractionation effects and exploration of new applications [J].Geostandards and Geoanalytical Research,2010,34:327-341.

    Arevalo R Jr, Bellucci J, McDonough W F. GGR bien-nial review: Advances in laser ablation and solution ICP-MS from 2008 to 2009 with particular emphasis on sensitivity enhancements, mitigation of fractionation effects and exploration of new applications [J].Geostandards and Geoanalytical Research,2010,34:327-341.
    Garcia C C, Wälle M, Lindner H, Koch J, Niemax K, Günther D. Femtosecnd laser ablation inductively coupled plasma mass spectrometry: Transport efficiencies of aerosols released under argon atmosphere and the importance of the focus position [J].Spectrochimica Acta: Part B,2008,63:271-276.

    Garcia C C, Wälle M, Lindner H, Koch J, Niemax K, Günther D. Femtosecnd laser ablation inductively coupled plasma mass spectrometry: Transport efficiencies of aerosols released under argon atmosphere and the importance of the focus position [J].Spectrochimica Acta: Part B,2008,63:271-276.
    Autrique D, Bogaerts A, Lindner H, Garcia C C, Niemax K. Design analysis of a laser ablation cell for inductively coupled plasma-mass spectrometry by numerical simulation [J].Spectrochimica Acta: Part B,2008,63:257-270.

    Autrique D, Bogaerts A, Lindner H, Garcia C C, Niemax K. Design analysis of a laser ablation cell for inductively coupled plasma-mass spectrometry by numerical simulation [J].Spectrochimica Acta: Part B,2008,63:257-270.
    Johnston S, Gehrels G, Valencia V, Ruiz J. Small volume U-Pb zircon geochronology by laser ablation-multicollector-ICP-MS [J].Chemical Geology,2009,259:218-229.

    Johnston S, Gehrels G, Valencia V, Ruiz J. Small volume U-Pb zircon geochronology by laser ablation-multicollector-ICP-MS [J].Chemical Geology,2009,259:218-229.
    李冰,杨红霞. 电感耦合等离子体质谱的原理和应用[M]. 北京:地质出版社,2005:74-84.
    Košler J, Sylvester P J. Present trends and the future of zircon in geochronology: Laser ablation ICPMS [J].Reviews in Mineralogy and Geochemistry,2003,53:243-275.

    Košler J, Sylvester P J. Present trends and the future of zircon in geochronology: Laser ablation ICPMS [J].Reviews in Mineralogy and Geochemistry,2003,53:243-275.
    Fernández B, Claverie F, Pécheyran C, Donard O F X. Direct analysis of solid samples by fs-LA-ICP-MS [J].Trends in Analytical Chemistry,2007,26(10):951-966.

    Fernández B, Claverie F, Pécheyran C, Donard O F X. Direct analysis of solid samples by fs-LA-ICP-MS [J].Trends in Analytical Chemistry,2007,26(10):951-966.
    Bleiner D, Günther D. Theoretical description and exp-erimental observation of aerosol transport processes in laser ablation inductively coupled plasma mass spectrometry [J].Journal of Analytical Atomic Spectrometry,2001,16:449-456.

    Bleiner D, Günther D. Theoretical description and exp-erimental observation of aerosol transport processes in laser ablation inductively coupled plasma mass spectrometry [J].Journal of Analytical Atomic Spectrometry,2001,16:449-456.
    Garcia C C, Lindner H, Niemax K. Transport efficiency in femtosecond laser ablation inductively coupled plasama mass spectrometry applying ablation cells with short and long washout times [J].Spectrochimica Acta: Part B,2007,62(1):13-19.

    Garcia C C, Lindner H, Niemax K. Transport efficiency in femtosecond laser ablation inductively coupled plasama mass spectrometry applying ablation cells with short and long washout times [J].Spectrochimica Acta: Part B,2007,62(1):13-19.
    Feldmann J, Kindness A, Ek P. Laser ablation of soft tissue using a cryogenically cooled ablation cell [J].Journal of Analytical Atomic Spectrometry,2002,17:813-818.

    Feldmann J, Kindness A, Ek P. Laser ablation of soft tissue using a cryogenically cooled ablation cell [J].Journal of Analytical Atomic Spectrometry,2002,17:813-818.
    Asogan D, Sharp B L, O'Connor C J P, Green D A, Hutchinson R W. An open, non-contact cell for laser ablation-inductively coupled plasma-mass spectrometry [J].Journal of Analytical Atomic Spectrometry,2009,24:917-923.

    Asogan D, Sharp B L, O'Connor C J P, Green D A, Hutchinson R W. An open, non-contact cell for laser ablation-inductively coupled plasma-mass spectrometry [J].Journal of Analytical Atomic Spectrometry,2009,24:917-923.
    Müller W, Shelley M, Miller P, Broude S. Initial performance metrics of a new custom-designed ArF excimer LA-ICPMS system coupled to a two-volume laser-ablation cell [J].Journal of Analytical Atomic Spectrometry,2009,24:209-214.

    Müller W, Shelley M, Miller P, Broude S. Initial performance metrics of a new custom-designed ArF excimer LA-ICPMS system coupled to a two-volume laser-ablation cell [J].Journal of Analytical Atomic Spectrometry,2009,24:209-214.
    Fricker M B, Kutscher D, Aeschlimann B, Frommer J, Dietiker R, Bettmer J, Günther D. High spatial resolution trace element analysis by LA-ICP-MS using a novel ablation cell for multiple or large samples [J].Intermational Journal of Mass Spectrometry,2011,307(1-3):39-45.

    Fricker M B, Kutscher D, Aeschlimann B, Frommer J, Dietiker R, Bettmer J, Günther D. High spatial resolution trace element analysis by LA-ICP-MS using a novel ablation cell for multiple or large samples [J].Intermational Journal of Mass Spectrometry,2011,307(1-3):39-45.
    Frei D, Gerdes A. Precise and accurate in situ U-Pb dating of zircon with high sample throughput by automated LA-SF-ICP-MS [J].Chemical Geology, 2009,261:261-270.

    Frei D, Gerdes A. Precise and accurate in situ U-Pb dating of zircon with high sample throughput by automated LA-SF-ICP-MS [J].Chemical Geology, 2009,261:261-270.
    Jackson S E, Pearson N J, Griffin W L, Belousova E A . The application of laser ablation-inductively coupled plasma-masss spectrometry to in situ U-Pb zircon geochronology [J].Chemical Geology,2004,211:47-69.

    Jackson S E, Pearson N J, Griffin W L, Belousova E A . The application of laser ablation-inductively coupled plasma-masss spectrometry to in situ U-Pb zircon geochronology [J].Chemical Geology,2004,211:47-69.
    Xia X P, Sun M, Zhao G C, Li H M, Zhou M F. Spot zircon U-Pb isotope analysis by ICP-MS coupled with a frequency quintupled(213 nm) Nd-YAG laser system [J]. Geochemical Journal,2004,38:191-200.

    Xia X P, Sun M, Zhao G C, Li H M, Zhou M F. Spot zircon U-Pb isotope analysis by ICP-MS coupled with a frequency quintupled(213 nm) Nd-YAG laser system [J]. Geochemical Journal,2004,38:191-200.
    Günther D, Heinrich C A. Comparison of the ablation behavior of 266 nm Nd: YAG and 193 nm ArF excimer lasers for LA-ICP-MS analysis [J].Journal of Analytical Atomic Spectrometry,1999,14:1369-1374.

    Günther D, Heinrich C A. Comparison of the ablation behavior of 266 nm Nd: YAG and 193 nm ArF excimer lasers for LA-ICP-MS analysis [J].Journal of Analytical Atomic Spectrometry,1999,14:1369-1374.
    Košler J, Wiedenbeck M, Wirth R, Hovorka J, Sylvester P , Míková J. Chemical and phase composition of particles produced by laser ablation of silicate glass and zircon-implications for elemental fractionation during ICP-MS analysis [J].Journal of Analytical Atomic Spectrometry,2005,20:402-409.

    Košler J, Wiedenbeck M, Wirth R, Hovorka J, Sylvester P , Míková J. Chemical and phase composition of particles produced by laser ablation of silicate glass and zircon-implications for elemental fractionation during ICP-MS analysis [J].Journal of Analytical Atomic Spectrometry,2005,20:402-409.
    Kuhn B K, Birbaum K, Luo Y, Günther D. Funda-mental studies on the ablation behaviour of Pb/U in NIST 610 and Zircon 91500 using laser ablation inductively coupled plasma mass spectrometry with respect to geochronology [J].Journal of Analytical Atomic Spectrometry,2010,25:21-27.

    Kuhn B K, Birbaum K, Luo Y, Günther D. Funda-mental studies on the ablation behaviour of Pb/U in NIST 610 and Zircon 91500 using laser ablation inductively coupled plasma mass spectrometry with respect to geochronology [J].Journal of Analytical Atomic Spectrometry,2010,25:21-27.
    Poitrasson F, Mao X L, Mao S S, Freydier R, Russo R E . Comparison of ultraviolet femtosecond and nanosecond laser ablation inductively coupled plasma mass spectrometry analysis in glass, monazite and zircon [J]. Analytical Chemistry,2003,75(22):6184-6190.

    Poitrasson F, Mao X L, Mao S S, Freydier R, Russo R E . Comparison of ultraviolet femtosecond and nanosecond laser ablation inductively coupled plasma mass spectrometry analysis in glass, monazite and zircon [J]. Analytical Chemistry,2003,75(22):6184-6190.
    Horn I, Blanckenbury F V. Investigation on elemental and isotopic fractionation during 196nm femtosecond laser ablation multiple collector inductively coupled plasma mass spectrometry [J].Spectrochimica Acta: Part B,2007,62:410-422.

    Horn I, Blanckenbury F V. Investigation on elemental and isotopic fractionation during 196nm femtosecond laser ablation multiple collector inductively coupled plasma mass spectrometry [J].Spectrochimica Acta: Part B,2007,62:410-422.
    Cottle J M, Horstwood M S A, Parrish R R. A new approach to single shot laser ablation analysis and its application to in situ Pb/U geochronology [J].Journal of Analytical Atomic Spectrometry,2009,24:1355-1363.

    Cottle J M, Horstwood M S A, Parrish R R. A new approach to single shot laser ablation analysis and its application to in situ Pb/U geochronology [J].Journal of Analytical Atomic Spectrometry,2009,24:1355-1363.
    Eggins S M, Kinsley L P J, Shelley J M G. Deposition and elemental fractionation processes during atmospheric pressure laser sampling for analysis by ICP-MS [J].Applied Surface Science,1998,127-129:278-286.

    Eggins S M, Kinsley L P J, Shelley J M G. Deposition and elemental fractionation processes during atmospheric pressure laser sampling for analysis by ICP-MS [J].Applied Surface Science,1998,127-129:278-286.
    Hu Z C, Gao S, Liu Y S, Hu S H, Chen H H, Yuan H L . Signal enhancement in laser ablation ICP-MS by addition of nitrogen in the central channel gas [J]. Journal of Analytical Atomic Spectrometry,2008,23:1093-1101.

    Hu Z C, Gao S, Liu Y S, Hu S H, Chen H H, Yuan H L . Signal enhancement in laser ablation ICP-MS by addition of nitrogen in the central channel gas [J]. Journal of Analytical Atomic Spectrometry,2008,23:1093-1101.
    Liu Y S, Hu Z C, Zong K Q, Gao C G, Gao S, Xu J, Chen H H. Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS [J].Chinese Science Bulletin,2010,55(15):1535-1546.

    Liu Y S, Hu Z C, Zong K Q, Gao C G, Gao S, Xu J, Chen H H. Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS [J].Chinese Science Bulletin,2010,55(15):1535-1546.
    Hirata T. Chemically assisted-laser ablation-ICP-mass spectrometry [J].Geochimica et Cosmochim Acta,2002, 66:A31.

    Hirata T. Chemically assisted-laser ablation-ICP-mass spectrometry [J].Geochimica et Cosmochim Acta,2002, 66:A31.
    Guillong M, Heinrich C A. Sensitivity enhancement in laser ablation ICP-MS using small amount of hydrogen in the carrier gas [J].Journal of Analytical Atomic Spectrometry,2007,22:1488-1494.

    Guillong M, Heinrich C A. Sensitivity enhancement in laser ablation ICP-MS using small amount of hydrogen in the carrier gas [J].Journal of Analytical Atomic Spectrometry,2007,22:1488-1494.
    Horn I, Rudnick R L, McDonough W F. Precise elem-ental and isotope ratio determination by simultaneous solution nebulization and laser abation-ICP-MS: Application to U-Pb geochronology [J].Chemical Geology,2000,164:281-301.

    Horn I, Rudnick R L, McDonough W F. Precise elem-ental and isotope ratio determination by simultaneous solution nebulization and laser abation-ICP-MS: Application to U-Pb geochronology [J].Chemical Geology,2000,164:281-301.
    柳小明,高山,第五春荣,袁洪林,胡兆初.单颗粒锆石的20μm小斑束原位微区LA-ICP-MS U-Pb年龄和微量元素的同时测定 [J].科学通报,2007,52(2):228-235.
    Feng R, Machado N, Ludden J. Lead geochronology of zircon by laserprobe-inductively coupled plasma-mass spectrometry(LP-ICP-MS) [J].Geochimica et Cosmochimica Acta,1993,57:3479-3486.

    Feng R, Machado N, Ludden J. Lead geochronology of zircon by laserprobe-inductively coupled plasma-mass spectrometry(LP-ICP-MS) [J].Geochimica et Cosmochimica Acta,1993,57:3479-3486.
    Hirata T, Nesbitt R W. U-Pb isotope geochronology of zircon: Evaluation of laser probe-inductively coupled plasma mass spectrometry technique [J].Geochimica et Cosmochimica Acta,1995,59:2491-2500.

    Hirata T, Nesbitt R W. U-Pb isotope geochronology of zircon: Evaluation of laser probe-inductively coupled plasma mass spectrometry technique [J].Geochimica et Cosmochimica Acta,1995,59:2491-2500.
    Košler J, Fonneland H, Sylvester P, Tubrett M, Pedersen R B . U-Pb dating of detrital zircons for sediment provenance studies—A comparison of laser ablation ICPMS and SIMS techniques [J].Chemical Geology,2002,182:605-618.

    Košler J, Fonneland H, Sylvester P, Tubrett M, Pedersen R B . U-Pb dating of detrital zircons for sediment provenance studies—A comparison of laser ablation ICPMS and SIMS techniques [J].Chemical Geology,2002,182:605-618.
    Wang Y, Fan W, Zhao G, Ji S, Peng T. Zircon U-Pb geochronology of gneissic rocks in the Yunkai massif and its implications on the Caledonian event in the South China Block [J].Gondwana Research,2007,12:404-416.

    Wang Y, Fan W, Zhao G, Ji S, Peng T. Zircon U-Pb geochronology of gneissic rocks in the Yunkai massif and its implications on the Caledonian event in the South China Block [J].Gondwana Research,2007,12:404-416.
    Cocheire A, Robert M. Laser ablation coupled with ICP-MS applied to U-Pb zircon geochronology: A review of recent advances [J].Gondwana Research,2008,14:597-608.

    Cocheire A, Robert M. Laser ablation coupled with ICP-MS applied to U-Pb zircon geochronology: A review of recent advances [J].Gondwana Research,2008,14:597-608.
    Jochum K P, Stoll B, Herwig K, Willbold M. Improve-ment of in situ Pb isotope analysis by LA-ICP-MS using 193nm Nd: YAG laser [J].Journal of Analytical Atomic Spectrometry,2006,21:666-675.

    Jochum K P, Stoll B, Herwig K, Willbold M. Improve-ment of in situ Pb isotope analysis by LA-ICP-MS using 193nm Nd: YAG laser [J].Journal of Analytical Atomic Spectrometry,2006,21:666-675.
    Gerdes A, Zeh A. Combined U-Pb and Hf isotope LA-(MC)-ICP-MS analyses of detrital zircons: Comparison with SHRIMP and new constraints for the provenance and age of an Armorican metasediment in Central Germany [J].Earth and Planetary Science Letters,2006,249:47-61.

    Gerdes A, Zeh A. Combined U-Pb and Hf isotope LA-(MC)-ICP-MS analyses of detrital zircons: Comparison with SHRIMP and new constraints for the provenance and age of an Armorican metasediment in Central Germany [J].Earth and Planetary Science Letters,2006,249:47-61.
    Janoušek V, Gerdes A, Vrána S, Finger F, Erban V, Friedl G, Braithwaite C R. Low-pressure granulites of the Lišov Massif, Southern Bohemia: Vis an metamorphism of Late Devonian plutonic arc rocks [J].Journal of Petrology,2006,47(4):705-744.

    Janoušek V, Gerdes A, Vrána S, Finger F, Erban V, Friedl G, Braithwaite C R. Low-pressure granulites of the Lišov Massif, Southern Bohemia: Vis an metamorphism of Late Devonian plutonic arc rocks [J].Journal of Petrology,2006,47(4):705-744.
    Polat A, Appel P W U, Frei R, Pan Y, Dilek Y, Ordó?ez-Calderón J C, Fryer B, Hollis J A, Raith J G. Field and geochemical characteristics of the Mesoarchean (~3075Ma) Ivisaartoq greenstone belt, southern West Greenland: Evidence for seafloor hydrothermal alteration in supra-subduction oceanic crust [J].Gondwana Research,2007,11:69-91.

    Polat A, Appel P W U, Frei R, Pan Y, Dilek Y, Ordó?ez-Calderón J C, Fryer B, Hollis J A, Raith J G. Field and geochemical characteristics of the Mesoarchean (~3075Ma) Ivisaartoq greenstone belt, southern West Greenland: Evidence for seafloor hydrothermal alteration in supra-subduction oceanic crust [J].Gondwana Research,2007,11:69-91.
    Gerdes A, Zeh A. Zircon formation versus zircon alteration—New insights from combined U-Pb and Lu-Hf in-situ LA-ICP-MS analyses and consequences for the interpretation of Archean zircon from the Central Zone of the Limpopo Belt [J].Chemical Geology,2009,261:230-243.

    Gerdes A, Zeh A. Zircon formation versus zircon alteration—New insights from combined U-Pb and Lu-Hf in-situ LA-ICP-MS analyses and consequences for the interpretation of Archean zircon from the Central Zone of the Limpopo Belt [J].Chemical Geology,2009,261:230-243.
    Willigers B J A, Baker J A, Krogstad E J, Peate D W. Precise and accurate in situ Pb-Pb dating of apatite, monazite and sphene by laser ablation multiple-collector ICP-MS [J].Geochimica et Cosmochimica Acta,2002,66(6):1051-1066.

    Willigers B J A, Baker J A, Krogstad E J, Peate D W. Precise and accurate in situ Pb-Pb dating of apatite, monazite and sphene by laser ablation multiple-collector ICP-MS [J].Geochimica et Cosmochimica Acta,2002,66(6):1051-1066.
    Horstwood M S A, Foster G L, Parrish R R, Noble S R, Nowell G N. Common-Pb corrected in situ U-Pb accessory mineral geochronology by LA-MC-ICP-MS [J].Journal of Analytical Atomic Spectrometry,2003,18:837-846.

    Horstwood M S A, Foster G L, Parrish R R, Noble S R, Nowell G N. Common-Pb corrected in situ U-Pb accessory mineral geochronology by LA-MC-ICP-MS [J].Journal of Analytical Atomic Spectrometry,2003,18:837-846.
    Simonetti A, Heaman L M, Hartlaub R P, Creaser R A, MacHattie T G, Böhm C. U-Pb zircon dating by laser ablation-MC-ICP-MS using a new multiple ion counting Faraday collector array [J].Journal of Analytical Atomic Spectrometry,2005,20:677-686.

    Simonetti A, Heaman L M, Hartlaub R P, Creaser R A, MacHattie T G, Böhm C. U-Pb zircon dating by laser ablation-MC-ICP-MS using a new multiple ion counting Faraday collector array [J].Journal of Analytical Atomic Spectrometry,2005,20:677-686.
    侯可军,李延河,田有荣. LA-MC-ICP-MS锆石微区原位U-Pb定年技术 [J].矿床地质,2009,28(4):481-492.
    Orihashi Y, Nakai S, Hirata T. U-Pb age determination for seven standard zircons using inductively coupled plasma-mass spectrometry coupled with frequency quintupled Nd-YAG(λ=213 nm) laser ablation syst-em: Comparison with LA-ICP-MS zircon analyses with a NIST glass reference material [J].Resource Geology,2008,58(2):101-103.

    Orihashi Y, Nakai S, Hirata T. U-Pb age determination for seven standard zircons using inductively coupled plasma-mass spectrometry coupled with frequency quintupled Nd-YAG(λ=213 nm) laser ablation syst-em: Comparison with LA-ICP-MS zircon analyses with a NIST glass reference material [J].Resource Geology,2008,58(2):101-103.
    Beintema K A, Mason P R D, Nelson D R, White S H, Wijbrans J R. New constraints on the timing of tectonic events in the Archaean Central Pilbara Craton, Western Australia[J]//Forster M A, Wijbrans J R. Geochronology and Structural Geology. Journal of the Virtual Explorer,2003,13(59).

    Beintema K A, Mason P R D, Nelson D R, White S H, Wijbrans J R. New constraints on the timing of tectonic events in the Archaean Central Pilbara Craton, Western Australia[J]//Forster M A, Wijbrans J R. Geochronology and Structural Geology. Journal of the Virtual Explorer,2003,13(59).
    Cox R A, Wilton D H C, Košler J. Laser-ablation U-Th-Pb in situ dating of zircon and allanite: An example from the October Harbour Granite, Central Coastal Labrador, Canada [J].The Canadian Mineralogist,2003,41(2):273-291.

    Cox R A, Wilton D H C, Košler J. Laser-ablation U-Th-Pb in situ dating of zircon and allanite: An example from the October Harbour Granite, Central Coastal Labrador, Canada [J].The Canadian Mineralogist,2003,41(2):273-291.
    Tiepolo M. In situ Pb geochronology zircon with laser ablation-inductively coupled plasma-sector field mass spectrometry [J].Chemical Geology,2003,199(1-2):159-177.

    Tiepolo M. In situ Pb geochronology zircon with laser ablation-inductively coupled plasma-sector field mass spectrometry [J].Chemical Geology,2003,199(1-2):159-177.
    Yuan H L, Gao S, Liu X M, Güther D, Wu F Y. Accurate U-Pb age and trace element determinations of zircon by laser ablation-inductively coupled plasma mass spectrometry [J].Geoanalytical and Geostandard Research,28(3):353-370.

    Yuan H L, Gao S, Liu X M, Güther D, Wu F Y. Accurate U-Pb age and trace element determinations of zircon by laser ablation-inductively coupled plasma mass spectrometry [J].Geoanalytical and Geostandard Research,28(3):353-370.
    Griffin W L, Belousova E A, Shee S R, Pearson N J, O'Reilly S Y. Archean crustal evolution in the northern Yilgarn Craton: U-Pb and Hf-isotope evidence from detrital zircons [J].Precambrian Research,2004,131(3-4):231-282.

    Griffin W L, Belousova E A, Shee S R, Pearson N J, O'Reilly S Y. Archean crustal evolution in the northern Yilgarn Craton: U-Pb and Hf-isotope evidence from detrital zircons [J].Precambrian Research,2004,131(3-4):231-282.
    Chang Z S, Vervoort J D, McClelland W C, Knaack C. U-Pb dating of zircon by LA-ICP-MS [J].Geochemistry Geophysics Geosystems,2006,7(5):1-14.

    Chang Z S, Vervoort J D, McClelland W C, Knaack C. U-Pb dating of zircon by LA-ICP-MS [J].Geochemistry Geophysics Geosystems,2006,7(5):1-14.
    谢烈文,张艳斌,张辉煌,孙金凤,吴福元.锆石/斜锆石 U-Pb和Lu-Hf同位素以及微量元素成分的同时原位测定 [J].科学通报,2008,53(2):220-228.
    Klötzli U, Klötzli E, Günes Z, Kosler J. Accuracy of laser ablation U-Pb zircon dating: Results from a test using five different reference zircons [J].Geostandards and Geoanalytical Research,2009,33:5-15.

    Klötzli U, Klötzli E, Günes Z, Kosler J. Accuracy of laser ablation U-Pb zircon dating: Results from a test using five different reference zircons [J].Geostandards and Geoanalytical Research,2009,33:5-15.
    Elhlou S, Belousova E A, Griffin W L, Pearson N J, O'Reilly S Y. Trace element and isotopic composition of GJ-red zircon standard by laser ablation [J].Geochimica et Cosmochimica Acta,2006,70(18):A158.

    Elhlou S, Belousova E A, Griffin W L, Pearson N J, O'Reilly S Y. Trace element and isotopic composition of GJ-red zircon standard by laser ablation [J].Geochimica et Cosmochimica Acta,2006,70(18):A158.
    Sláma J, Košler J, Condon D J, Crowley J L, Gerdes A, Hanchar J M, Horstwood M S A, Morris G A, Nasdala L, Norberg N, Schaltegger U, Schoene B. Plešovice zircon—A new natural reference material for U-Pb and Hf isotopic microanalysis [J].Chemical Geology,2008,249:1-35.

    Sláma J, Košler J, Condon D J, Crowley J L, Gerdes A, Hanchar J M, Horstwood M S A, Morris G A, Nasdala L, Norberg N, Schaltegger U, Schoene B. Plešovice zircon—A new natural reference material for U-Pb and Hf isotopic microanalysis [J].Chemical Geology,2008,249:1-35.
    袁洪林,吴福元,高山,柳小明,徐平,孙德有.中国东部新生代侵入体的锆石激光探针年龄测定与稀土元素成分分析:对渐新世幔源岩浆底侵作用和地壳抬升的指示 [J].科学通报,2003,48(14):1511-1520.
    Black L P, Kamo S L, Allen C M, Davis D W, Aleiniknoff J N, Valley J W, Mundil R, Campbell I H, Korsch R J, Williams I S, Foudoulis C. Improved 206Pb/238U microprobe geochronology by the monitoring of a trace-element-related matrix effect; SHRIMP, ID-TIMS, ELA-ICP-MS and oxygen isotope documentation for a series of zircon standards [J].Chemical Geology,2004,205(1-2):115-140.

    Black L P, Kamo S L, Allen C M, Davis D W, Aleiniknoff J N, Valley J W, Mundil R, Campbell I H, Korsch R J, Williams I S, Foudoulis C. Improved 206Pb/238U microprobe geochronology by the monitoring of a trace-element-related matrix effect; SHRIMP, ID-TIMS, ELA-ICP-MS and oxygen isotope documentation for a series of zircon standards [J].Chemical Geology,2004,205(1-2):115-140.
    Wiedenbeck M, Alle P, Corfu F, Griffin W L, Meier M, Oberli F, Von Quadt A, Roddick J C, Spiegel W. Three natural zircon standards for U-Th-Pb, Lu-Hf, trace element and REE analyses [J].Geostandards Newsletter,1995,19(1):1-23.

    Wiedenbeck M, Alle P, Corfu F, Griffin W L, Meier M, Oberli F, Von Quadt A, Roddick J C, Spiegel W. Three natural zircon standards for U-Th-Pb, Lu-Hf, trace element and REE analyses [J].Geostandards Newsletter,1995,19(1):1-23.
    Wiedenbeck M, Hanchar J M, Peck W H, Sylvester P, Valley J, Whitehouse M, Kronz A, Morishita Y, Nasdala L. Further characterization of the 91500 zircon crystal [J].Geostandards and Geoanalytical Research,2004,28:9-39.

    Wiedenbeck M, Hanchar J M, Peck W H, Sylvester P, Valley J, Whitehouse M, Kronz A, Morishita Y, Nasdala L. Further characterization of the 91500 zircon crystal [J].Geostandards and Geoanalytical Research,2004,28:9-39.
    Lopez R, Cameron K L, Jones N W. Evidence for Paleoproterozoic, Grenvillian and Pan-African age Gondwana crust beneath north-eastern Mexico [J].Precambiran Research,2001,107:195-214.

    Lopez R, Cameron K L, Jones N W. Evidence for Paleoproterozoic, Grenvillian and Pan-African age Gondwana crust beneath north-eastern Mexico [J].Precambiran Research,2001,107:195-214.
    Paquette J L, Pin C. A new miniaturized extraction chro-matography method for precise U-Pb zircon geochronology [J].Chemical Geology,2001,176:311-319.

    Paquette J L, Pin C. A new miniaturized extraction chro-matography method for precise U-Pb zircon geochronology [J].Chemical Geology,2001,176:311-319.
    Amelin Y V, Zaitsev A N. Precise geochronology of phos-corites and carbonatites: The critical role of U-series disequilirium in age interpretations [J].Geochimica et Cosmochimica Acta,2002,66:2399-2419.

    Amelin Y V, Zaitsev A N. Precise geochronology of phos-corites and carbonatites: The critical role of U-series disequilirium in age interpretations [J].Geochimica et Cosmochimica Acta,2002,66:2399-2419.
    Chen F, Siebel W, Satir M. Zircon U-Pb and Pb isotope fractionation during stepwise HF acid leaching and geochronological implications [J].Chemical Geology,2002,191:155-164.

    Chen F, Siebel W, Satir M. Zircon U-Pb and Pb isotope fractionation during stepwise HF acid leaching and geochronological implications [J].Chemical Geology,2002,191:155-164.
    Nebel-Jacobsen Y, Scherer E E, Munker C, Mezger K. Separation of U, Pb, Lu and Hf from single zircons for combined U-Pb dating and Hf isotope measurements by TIMS and MC-ICPMS [J].Chemical Geology,2001,176:311-319.

    Nebel-Jacobsen Y, Scherer E E, Munker C, Mezger K. Separation of U, Pb, Lu and Hf from single zircons for combined U-Pb dating and Hf isotope measurements by TIMS and MC-ICPMS [J].Chemical Geology,2001,176:311-319.
    Nasdala L, Hofmeister W, Norberg N, Mattinson J M, Corfu F, Dörr W, Kamo S L, Kennedy A K, Kronz A, Reiners P W, Frei D, Kosler J, Wan Y, Götze J, Häger T, Kröner A, Valley J W. Zircon M257—A homogeneous natural reference material for the ion microprobe U-Pb analysis of zircon [J].Geostandards and Geoanalytical Research,2008,32:247-265.

    Nasdala L, Hofmeister W, Norberg N, Mattinson J M, Corfu F, Dörr W, Kamo S L, Kennedy A K, Kronz A, Reiners P W, Frei D, Kosler J, Wan Y, Götze J, Häger T, Kröner A, Valley J W. Zircon M257—A homogeneous natural reference material for the ion microprobe U-Pb analysis of zircon [J].Geostandards and Geoanalytical Research,2008,32:247-265.
    Black L P, Kamo S L, Allen C M, Aleinikoff J N, Davis D W, Korsch R J, Foudoulis C. TEMORA 1: A new zircon standard for Phanerozoic U-Pb geochronology [J].Chemical Geology,2003,200:155-170.

    Black L P, Kamo S L, Allen C M, Aleinikoff J N, Davis D W, Korsch R J, Foudoulis C. TEMORA 1: A new zircon standard for Phanerozoic U-Pb geochronology [J].Chemical Geology,2003,200:155-170.
    Black L P, Kamo S L, Williams I S, Mundil R, Davis D W, Korsch R J, Foudoulis C. The application of SHRIMP to Phanerozoic geochronology: A critical appraisal of four zircon standards [J].Chemical Geology,2003,200:171-188.

    Black L P, Kamo S L, Williams I S, Mundil R, Davis D W, Korsch R J, Foudoulis C. The application of SHRIMP to Phanerozoic geochronology: A critical appraisal of four zircon standards [J].Chemical Geology,2003,200:171-188.
    Li X H, Liu Y, Li Q L, Guo C H. Precise determination of Phanerozoic zircon Pb/Pb age by multicollector SIMS without external standardization [J].Geochemistry Geophysics Geosystems,2009,10(4):1-21.

    Li X H, Liu Y, Li Q L, Guo C H. Precise determination of Phanerozoic zircon Pb/Pb age by multicollector SIMS without external standardization [J].Geochemistry Geophysics Geosystems,2009,10(4):1-21.
    Claou-Long J C, Compston W, Roberts J, Fanning C M. Two carboniferous ages: A comparison of SHRIMP zircon dating with conventional zircon ages and 40Ar/39Ar analysis[M]//Berggren W A, Kent D V, Aubrey M P, Hardenbol J, eds. Geochronology time scales and global stratugraphic correlation: SEPM (Society for Sedimentary Geology).Special Publication.1995,54:3-21.

    Claou-Long J C, Compston W, Roberts J, Fanning C M. Two carboniferous ages: A comparison of SHRIMP zircon dating with conventional zircon ages and 40Ar/39Ar analysis[M]//Berggren W A, Kent D V, Aubrey M P, Hardenbol J, eds. Geochronology time scales and global stratugraphic correlation: SEPM (Society for Sedimentary Geology).Special Publication.1995,54:3-21.
    Roddick J C, van Breemen O. U-Pb zircon dating: A comparison of ion microprobe and single grain conventional analyses. Radiogenic age and isotopic studies: Report 8 Geological Survey of Canada[J].Current Research,1994,F:1-9.

    Roddick J C, van Breemen O. U-Pb zircon dating: A comparison of ion microprobe and single grain conventional analyses. Radiogenic age and isotopic studies: Report 8 Geological Survey of Canada[J].Current Research,1994,F:1-9.
    Takahata N, Tsutsumi Y, Sano Y. Ion microprobe U-Pb dating of zircon with a 15 micrometer spatial resolution using NanoSIMS [J].Gondwana Research,2008,14:587-596.

    Takahata N, Tsutsumi Y, Sano Y. Ion microprobe U-Pb dating of zircon with a 15 micrometer spatial resolution using NanoSIMS [J].Gondwana Research,2008,14:587-596.
    Mortimer G E, Cooper J A, Oliver R L. The geochem-ical evolution of Proterozoic granitoids near Port Lincoln in the Gawler Orogenic Domain of South Australia [J].Precambrian Research,1988,40/41:387-406.

    Mortimer G E, Cooper J A, Oliver R L. The geochem-ical evolution of Proterozoic granitoids near Port Lincoln in the Gawler Orogenic Domain of South Australia [J].Precambrian Research,1988,40/41:387-406.
    Daly S L, Fannning C M, Fairclough M C. Tectonic evolution and exploration potential of the Gawler Craton, South Australia [J].Journal of Australian Geology and Geophysics,1988,17:145-168.

    Daly S L, Fannning C M, Fairclough M C. Tectonic evolution and exploration potential of the Gawler Craton, South Australia [J].Journal of Australian Geology and Geophysics,1988,17:145-168.
    Dougherty-Page J S, Bartlett J M. New analytical proce-dures to increase the resolution of zircon geochronology by the evaporation technique [J].Chemical Geology,1999,153:227-240.

    Dougherty-Page J S, Bartlett J M. New analytical proce-dures to increase the resolution of zircon geochronology by the evaporation technique [J].Chemical Geology,1999,153:227-240.
    Paces J B, Miller J D. Precise U-Pb ages of Duluth complex and related mafic intrusions, northeastern Minnesota: Geochronological insights into physical, petrogenetic, paleomagnetic, and tectonomagmatic processes associated with the 1.1 Ga midcontinent rift system [J].Journal of Geophysical Research,1993,98:13997-14013.

    Paces J B, Miller J D. Precise U-Pb ages of Duluth complex and related mafic intrusions, northeastern Minnesota: Geochronological insights into physical, petrogenetic, paleomagnetic, and tectonomagmatic processes associated with the 1.1 Ga midcontinent rift system [J].Journal of Geophysical Research,1993,98:13997-14013.
    Schmitz M D, Bowring S A, Ireland T R. Evaluation of duluth complex anorthositic series(AS3) zircon as a U-Pb geochronological standard: New high-precision isotope dilution thermal ionization mass spectrometry results [J].Geochimica et Cosmochimica Acta,2003,67(19):3665-3672.

    Schmitz M D, Bowring S A, Ireland T R. Evaluation of duluth complex anorthositic series(AS3) zircon as a U-Pb geochronological standard: New high-precision isotope dilution thermal ionization mass spectrometry results [J].Geochimica et Cosmochimica Acta,2003,67(19):3665-3672.
    Fisher C M, Longerich H P, Jackson S E, Hanchar J M. Data acquisition and calculation of U-Pb isotopic analyses using laser ablation (single collector) inductively coupled plasma mass spectrometry [J].Journal of Analytical Atomic Spectrometry,2010, 25:1905-1920.

    Fisher C M, Longerich H P, Jackson S E, Hanchar J M. Data acquisition and calculation of U-Pb isotopic analyses using laser ablation (single collector) inductively coupled plasma mass spectrometry [J].Journal of Analytical Atomic Spectrometry,2010, 25:1905-1920.
    Williams I S. U-Th-Pb geochronology by ion microprobe[M]//Mckibben M A, Shanks Ⅲ W C, Ridley W I, eds. Applications of microanalytical techniques to understanding mineralizing processes.Society of Economic Geologists,1998:1-35.

    Williams I S. U-Th-Pb geochronology by ion microprobe[M]//Mckibben M A, Shanks Ⅲ W C, Ridley W I, eds. Applications of microanalytical techniques to understanding mineralizing processes.Society of Economic Geologists,1998:1-35.
    Compston W, Williams I S, Meyer C. U-Pb geochro-nology of zircons from lunar breccia 73217 using a sentitive high mass-resolution ion microprobe [J].Journal of Geophysical Research,1984,89:B525-B534.

    Compston W, Williams I S, Meyer C. U-Pb geochro-nology of zircons from lunar breccia 73217 using a sentitive high mass-resolution ion microprobe [J].Journal of Geophysical Research,1984,89:B525-B534.
    Williams I S, Buick I S, Cartwright I. An extended episode of early mesoproterozoic metamorphic fluid flow in the Reynolds range, central Australia [J].Journal of Metamorphical Geology,1996,14:29-47.

    Williams I S, Buick I S, Cartwright I. An extended episode of early mesoproterozoic metamorphic fluid flow in the Reynolds range, central Australia [J].Journal of Metamorphical Geology,1996,14:29-47.
    Doe B R, Stacey J S. The application of lead isotopes to the problems of ore genesis and ore prospect evoluation: A review [J].Economic Geology,1974,69:757-776.

    Doe B R, Stacey J S. The application of lead isotopes to the problems of ore genesis and ore prospect evoluation: A review [J].Economic Geology,1974,69:757-776.
    Stacy J S, Kramers J D. Approximation of terrestrial lead isotope evolution by a two-stage model [J]. Earth and Planetary Science Letters,1975,26:207-221.

    Stacy J S, Kramers J D. Approximation of terrestrial lead isotope evolution by a two-stage model [J]. Earth and Planetary Science Letters,1975,26:207-221.
    Anderson T. Correction of common lead in U-Pb ana-lyses that do not report 204Pb [J].Chemical Geology,2002,192:59-79.

    Anderson T. Correction of common lead in U-Pb ana-lyses that do not report 204Pb [J].Chemical Geology,2002,192:59-79.
    Li X H, Liang X R, Sun M, Liu Y, Tu X L. Geochronology and geochemistry of single-grain zircons: Simultaneous in-situ analysis of U-Pb age and trace elements by LAM-ICP-MS [J].European Journal of Mineralogy,2000,12:1015-1024.

    Li X H, Liang X R, Sun M, Liu Y, Tu X L. Geochronology and geochemistry of single-grain zircons: Simultaneous in-situ analysis of U-Pb age and trace elements by LAM-ICP-MS [J].European Journal of Mineralogy,2000,12:1015-1024.
    Iizuka T, Horata T. Simultaneous determinations of U-Pb age and REE abundances for zircons using ArF excimer laser ablation-ICPMS [J].Geochemical Journal,2004,38:229-241.

    Iizuka T, Horata T. Simultaneous determinations of U-Pb age and REE abundances for zircons using ArF excimer laser ablation-ICPMS [J].Geochemical Journal,2004,38:229-241.
    Hu Z C, Liu Y S, Chen L, Zhou L, Li M, Zong K Q, Zhu L Y, Gao S. Contrasting matrix induced elemental fractionation in NIST SRM and rock glasses during laser ablation ICP-MS analysis at high spatial resolution [J].Journal of Analytical Atomic Spectrometry,2011,26:425-430.

    Hu Z C, Liu Y S, Chen L, Zhou L, Li M, Zong K Q, Zhu L Y, Gao S. Contrasting matrix induced elemental fractionation in NIST SRM and rock glasses during laser ablation ICP-MS analysis at high spatial resolution [J].Journal of Analytical Atomic Spectrometry,2011,26:425-430.
    Yuan H L, Gao S, Dai M N, Zong C L, Günther D, Fontaine G H, Liu X M, Diwu C R. Simultaneous determinations of U-Pb age, Hf isotopes and trace element compositions of zircon by excimer laser-ablation quadrupole and multiple-collector ICP-MS [J].Chemical Geology,2008,247:100-118.

    Yuan H L, Gao S, Dai M N, Zong C L, Günther D, Fontaine G H, Liu X M, Diwu C R. Simultaneous determinations of U-Pb age, Hf isotopes and trace element compositions of zircon by excimer laser-ablation quadrupole and multiple-collector ICP-MS [J].Chemical Geology,2008,247:100-118.
    Dodson M H, Compston W, Williams I S, Wilson J F. A search for ancient detrital zircons from Zimbabwan sediments [J].Journal of the Geological Society,1988,145:977-983.

    Dodson M H, Compston W, Williams I S, Wilson J F. A search for ancient detrital zircons from Zimbabwan sediments [J].Journal of the Geological Society,1988,145:977-983.
    Machado N, Gauthier G. Determination of 207Pb/206Pb ages on zircon and monazite by laser ablation ICPMS and application to a study of sedimentary provenance and metamorphism in southeastern Brazil [J].Geochimica et Cosmochimica Acta, 1996,60:5063-5073.

    Machado N, Gauthier G. Determination of 207Pb/206Pb ages on zircon and monazite by laser ablation ICPMS and application to a study of sedimentary provenance and metamorphism in southeastern Brazil [J].Geochimica et Cosmochimica Acta, 1996,60:5063-5073.
    李秋根,刘树文,王宗起,张帆,陈友章,王涛.中条山绛县群碎屑锆石LA-ICP-MS U-Pb测年及其地质意义[J].岩石学报,2008,24(6):1359-1368.
    王节涛,李长安,杨勇,王秋良.江汉平原周老孔中碎屑锆石LA-ICP-MS定年及物源示踪 [J].第四纪研究,2009,29(2):343-350.
    刘建辉,刘敦一,张玉海,杨之青.使用SHRIMP测定锆石铀-铅年龄的选点技巧 [J].岩矿测试,2011,30(3):265-268.
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