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WEI Jing-jing, XUE Qiu-hong, LIU Xin-tong, SHAN Bao-tian, DING Yu-long. Determination of 15 Impurity Elements in Quartz Sand by Inductively Coupled Plasma-Atomic Emission Spectrometry[J]. Rock and Mineral Analysis, 2011, 30(3): 310-314.
Citation: WEI Jing-jing, XUE Qiu-hong, LIU Xin-tong, SHAN Bao-tian, DING Yu-long. Determination of 15 Impurity Elements in Quartz Sand by Inductively Coupled Plasma-Atomic Emission Spectrometry[J]. Rock and Mineral Analysis, 2011, 30(3): 310-314.
shu

Determination of 15 Impurity Elements in Quartz Sand by Inductively Coupled Plasma-Atomic Emission Spectrometry

  • 1.

    College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao 266003, China

  • 2.

    Shandong Entry-Exit Inspection and Quarantine Bureau, Qingdao 266002, China

  • 3.

    Shandong Entry-Exit Inspection and Quarantine Bureau, Qingdao 266002, China

  • 4.

    Shandong Entry-Exit Inspection and Quarantine Bureau, Qingdao 266002, China

  • 5.

    College of Chemistry and Chemical Engineering, Ocean University of China, Qingdao 266003, China

  • 6.

    Shandong Entry-Exit Inspection and Quarantine Bureau, Qingdao 266002, China

More Information
  • Received Date: August 10, 2010
  • Revised Date: January 16, 2011
    Abstract
  • A method was developed to determine of Fe, Ti, Mg, Mn, Zn, Cu, Pb, As, Cd, Ni, Cr, Co, Sb, Al and Ba in the quartz sand by inductively coupled plasma-atomic emission spectrometry (ICP-AES). The effect of the HF-HClO4 and HF-H2SO4 digestion systems to the results was investigated. Moreover, the conditions of acid consumption, digestion temperature and instrumental conditions were optimized. The detection limits for the elements were 0.17-0.88 μg/g and the recoveries of the method were 90.4%-110.7% with RSD (n=6) of less than 5.0%. The method possesses the advantages of simple operation, high sensitivity, good precision and is suitable for routine analysis of impurity elements in the quartz sand.
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    • References (24)
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