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ZHOU Jiao-hua, WANG Jian-yu, ZHONG Li-xiang, CHEN Hao-feng, WANG Yu-lin. Determination of Selenium in Biological Samples by Hydride Generation- Atomic Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2011, 30(2): 214-216.
Citation: ZHOU Jiao-hua, WANG Jian-yu, ZHONG Li-xiang, CHEN Hao-feng, WANG Yu-lin. Determination of Selenium in Biological Samples by Hydride Generation- Atomic Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2011, 30(2): 214-216.
shu

Determination of Selenium in Biological Samples by Hydride Generation- Atomic Fluorescence Spectrometry

  • 1.

    The Geoanalysis Laboratory of Henan Province, Zhengzhou 450012, China

  • 2.

    China Gold Science and Technology CO., LTD, Beijing 100176, China

  • 3.

    The Geoanalysis Laboratory of Henan Province, Zhengzhou 450012, China

  • 4.

    The Geoanalysis Laboratory of Henan Province, Zhengzhou 450012, China

  • 5.

    The 3rd Geological Survey Team, Geological Exploration Bureau of Henan Province, Xinyang 464000, China

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  • Received Date: April 29, 2010
  • Revised Date: July 11, 2010
    Abstract
  • A method for determination of selenium in biological samples by hydride generation-atomic fluorescence spectrometry was developed. The samples were decomposed with HNO3-HClO4 and Fe3+ was used as relieving reagent in 4 mol/L HCl medium. The detection limit of the method was 0.02 μg/L. The method has been applied to the determination of selenium in biological national standard reference materials and the results are in agreement with certified values with precision of 1.51% RSD(n=11).
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    • References (15)
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