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LI Song, RAO Zhu. Determination of Benz(a)Pyrene in Groundwaters by Ultra Performance Liquid Chromatography[J]. Rock and Mineral Analysis, 2010, 29(6): 679-682.
Citation: LI Song, RAO Zhu. Determination of Benz(a)Pyrene in Groundwaters by Ultra Performance Liquid Chromatography[J]. Rock and Mineral Analysis, 2010, 29(6): 679-682.

Determination of Benz(a)Pyrene in Groundwaters by Ultra Performance Liquid Chromatography

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  • Received Date: January 17, 2010
  • Revised Date: April 29, 2010
  • A simple method for the determination of benz(a)pyrene in groundwater by ultra performance liquid chromatography was developed. The method was discussed for the wavelength of fluorescence absorbance detection and the temperature of chromatographic column. The separation was carried out on Acquity C18 column with methanol as the mobile phase at a constant flow rate of 0.40 mL/min. Linear detection response was obtained for concentrations ranging from 0.082 to 200 ng/mL.The limit of detection was 0.033 ng/mL. The retention time of benz(a)pyrene is 0.61 min. The ultra performance liquid chromatography and high performance liquid chromatography method was compared to detect the benz(a)pyrene in this paper. This technology, ultra performance liquid chromatography, has significant theoretical advantages in speed, resolution, and sensitivity of analysis, especially time saving and solvent consumption.
  • 饶竹,李松,何淼,苏劲.高效液相色谱-荧光-紫外串联测定土壤中16种多环芳烃[J].分析化学,2007,35(7):954-958.
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    Park Daejin, Phapale Prasadb, Jang Injin, Cui Song, Moon Byungjo, Kim Jungeun, Kim Woomi, Hwang Sungkyu, Yoon Youngran. An Improved UPLC method for rapid analysis of levofloxacin in human plasma[J]. Chromatographia, 2008,68:187-192.

    Park Daejin, Phapale Prasadb, Jang Injin, Cui Song, Moon Byungjo, Kim Jungeun, Kim Woomi, Hwang Sungkyu, Yoon Youngran. An Improved UPLC method for rapid analysis of levofloxacin in human plasma[J]. Chromatographia, 2008,68:187-192.
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    Citov I, Havl kov L, Urb nek L, Solichov D, Nov kov L, Solich P. Comparison of a novel ultra-performance liquid chromatographic method for determination of retinol and α-tocopherol in human serum with conventional HPLC using monolithic and particulate columns[J]. Analytical and Bioanalytical Chemistry,2007,388:675-681.
    [JP2]Ates Z, Özden T, Özilhan S, Toptan S. Simultaneous determination of carbamazepine and its active metabolite carbamazepine-10,11-epoxide in human plasma by UPLC[J]. Chromatographia,2007,66:123-127.

    [JP2]Ates Z, Özden T, Özilhan S, Toptan S. Simultaneous determination of carbamazepine and its active metabolite carbamazepine-10,11-epoxide in human plasma by UPLC[J]. Chromatographia,2007,66:123-127.
    Güvenç A, Şatr E, Coşkun M. Determination of ruscogenin in Turkish Ruscus L. species by UPLC[J].Chromatographia,2007,66:141-145.

    Güvenç A, Şatr E, Coşkun M. Determination of ruscogenin in Turkish Ruscus L. species by UPLC[J].Chromatographia,2007,66:141-145.
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    Zhou Jinhui, Zhao Jing, Yuan Hancheng, Meng Ying, Li Yi, Wu Liming, Xue Xiaofeng. Comparison of UPLC and HPLC for determination of trans-10-hydroxy-2-decenoic acid content in royal jelly by ultrasound-assisted extraction with internal standard[J]. Chromatographia,2007,66:185-190.
    Chauveau Duriot B, Doreau M, Nozière P, Graulet B. Simultaneous quantification of carotenoids, retinol, and tocopherols in forages, bovine plasma, and milk: Validation of a novel UPLC method[J]. Analytical and Bioanalytical Chemistry,2010,397:777-790.

    Chauveau Duriot B, Doreau M, Nozière P, Graulet B. Simultaneous quantification of carotenoids, retinol, and tocopherols in forages, bovine plasma, and milk: Validation of a novel UPLC method[J]. Analytical and Bioanalytical Chemistry,2010,397:777-790.
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    Wang Yuefei, Wu Bin, Yang Jing, Hu Limin, Su Yanfang, Gao Xiumei. A rapid method for the analysis of ten compounds in Psoralea corylifolia L. by UPLC[J]. Chromatographia, 2009,70:199-204.
    Mariateresa Maldini, Paola Montoro, Ireneusz Kapusta, Wieslaw Oleszek, Sonia Piacente, Cosimo Pizza. Quantitative analysis of caffeoylquinic acids and styryl-pyrones in Sweetia Panamensis Bark by UPLC[J].Chromatographia,2009,70:1621-1626.

    Mariateresa Maldini, Paola Montoro, Ireneusz Kapusta, Wieslaw Oleszek, Sonia Piacente, Cosimo Pizza. Quantitative analysis of caffeoylquinic acids and styryl-pyrones in Sweetia Panamensis Bark by UPLC[J].Chromatographia,2009,70:1621-1626.
    Manabu Nakazono, Yasuyuki Sato, Shigeo Hasegawa, Norimasa Arisuda, Aiko Miyamoto, Kiyoshi Zaitsu. Rapid separation of hydrophobic compounds by UPLC: In case of bisindolylmaleimides, indolocarbazoles or fullerene C60 derivatives[J].Chromatographia, 2009,70:933-937.

    Manabu Nakazono, Yasuyuki Sato, Shigeo Hasegawa, Norimasa Arisuda, Aiko Miyamoto, Kiyoshi Zaitsu. Rapid separation of hydrophobic compounds by UPLC: In case of bisindolylmaleimides, indolocarbazoles or fullerene C60 derivatives[J].Chromatographia, 2009,70:933-937.
    Giedr Kesiūnait , AuŠra Linkevi iūt , Evaldas Naujalis, Audrius Padarauskas. Matrix solid-phase dispersion extraction and UPLC determination of Sudan dyes in Chili Powder[J].Chromatographia,2009,70:1691-1695.

    Giedr Kesiūnait , AuŠra Linkevi iūt , Evaldas Naujalis, Audrius Padarauskas. Matrix solid-phase dispersion extraction and UPLC determination of Sudan dyes in Chili Powder[J].Chromatographia,2009,70:1691-1695.
    Wu Ting, Wang Chao, Wang Xing, Xiao Haiqing, Ma Qiang, Zhang Qing. Comparison of UPLC and HPLC for analysis of 12 phthalates[J].Chromatographia,2008,68:803-806.

    Wu Ting, Wang Chao, Wang Xing, Xiao Haiqing, Ma Qiang, Zhang Qing. Comparison of UPLC and HPLC for analysis of 12 phthalates[J].Chromatographia,2008,68:803-806.
    李松,饶竹.地下水中12项半挥发性有机污染物测定的质量控制[J].岩矿测试,2009, 28(2): 157-160.
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