Determination of 16 Polycyclic Aromatic Hydrocarbons in Soils by Gas Chromatography-Mass Spectrometry

ZHANG Xiao-hui; WANG Xiao-yan

Rock and Mineral Analysis > 2010 > 29(5): 535-538.

ZHANG Xiao-hui, WANG Xiao-yan. Determination of 16 Polycyclic Aromatic Hydrocarbons in Soils by Gas Chromatography-Mass Spectrometry[J]. Rock and Mineral Analysis, 2010, 29(5): 535-538.

Citation:

ZHANG Xiao-hui, WANG Xiao-yan. Determination of 16 Polycyclic Aromatic Hydrocarbons in Soils by Gas Chromatography-Mass Spectrometry[J]. Rock and Mineral Analysis, 2010, 29(5): 535-538.

Citation:

ZHANG Xiao-hui, WANG Xiao-yan. Determination of 16 Polycyclic Aromatic Hydrocarbons in Soils by Gas Chromatography-Mass Spectrometry[J]. Rock and Mineral Analysis, 2010, 29(5): 535-538.

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Determination of 16 Polycyclic Aromatic Hydrocarbons in Soils by Gas Chromatography-Mass Spectrometry

1.
Shannxi Institute of Geoanalysis, Xi'an 710054, China
2.
Shannxi Institute of Geoanalysis, Xi'an 710054, China

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Received Date: January 17, 2010
Revised Date: April 26, 2010

Abstract

ABSTRACT

A method for the determination of 16 polycyclic aromatic hydrocarbons (PAHs) in soils by gas chromatography-mass spectrometry (GC-MS) with accelerated solvent extraction (ASE) sample preparation was developed. A mixture solution of methylene chloride/acetone (1∶1, V/V) was selected as the optimum extraction solvent through the experiments. The detection limits of the method for PAHs were 0.10~3.9 ng/g and the recoveries were 72.6%~123.5%. The method provides the advantages of lower detection limits, good precision and is suitable for the determination of PAHs in soils.
- accelerated,
- solvent,
- extraction,
- gas

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