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MA Han-yu, LIU Fei, LIU Yu-long. Determination of Organochlorine Pesticides and Polychlorinated Biphenyls in Groundwater by Gas Chromatography[J]. Rock and Mineral Analysis, 2010, 29(5): 527-530.
Citation: MA Han-yu, LIU Fei, LIU Yu-long. Determination of Organochlorine Pesticides and Polychlorinated Biphenyls in Groundwater by Gas Chromatography[J]. Rock and Mineral Analysis, 2010, 29(5): 527-530.

Determination of Organochlorine Pesticides and Polychlorinated Biphenyls in Groundwater by Gas Chromatography

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  • Received Date: January 17, 2010
  • Revised Date: June 02, 2010
  • A method for the determination of common organochlorine pesticides (OCPs) and polychlorinated biphenyls (PCBs) in groundwater by gas chromatography (GC) was developed. The method provides the detection limits of lower than 2.21 ng/L for OCPs, 5.20 ng/L for PCB 1 and lower than 1.30 ng/L for other target pollutants. The recoveries for most of the OCPs and PCBs were 63.5%~110.2% with precision of 2.2%~17.3% RSD (n=5) and the recoveries of the pollutants in practical samples were 87.34%~133.76% except for endrin. The method provides the advantages of good stability and reproducibility, simple sample preparation and has been applied to the determination of OCPs and PCBs in groundwater samples.
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    EPA Method 8081B,Oraganochlorine pesticides by gas chromatography[S].

    EPA Method 8081B,Oraganochlorine pesticides by gas chromatography[S].
    EPA Method 8082A,Polychlorinated biphenyls by gas chromatography[S].

    EPA Method 8082A,Polychlorinated biphenyls by gas chromatography[S].
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    Chen F,Chen L,Wang Q,Zhou J,Xue X,Zhao J. Determination of organochlorine pesticides in propolis by gas chromatography-electron capture detection using double column series solid-phase extraction[J]. Analytical and Bioanalytical Chemistry,2009,393:1073-1079.
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    Farahania H, Yaminia Y, Shariatib S, Khalili-Zanjania M R, Mansour-Baghahic S. Development of liquid phase microextraction method based on solidification of floated organic drop for extraction and preconcentration of organochlorine pesticides in water samples[J].Analytica Chimica Acta,2008,626(2):166-173.
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