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MA Han-yu, LIU Fei, LIU Yu-long. Determination of Organochlorine Pesticides and Polychlorinated Biphenyls in Groundwater by Gas Chromatography[J]. Rock and Mineral Analysis, 2010, 29(5): 527-530.
Citation: MA Han-yu, LIU Fei, LIU Yu-long. Determination of Organochlorine Pesticides and Polychlorinated Biphenyls in Groundwater by Gas Chromatography[J]. Rock and Mineral Analysis, 2010, 29(5): 527-530.

Determination of Organochlorine Pesticides and Polychlorinated Biphenyls in Groundwater by Gas Chromatography

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  • Received Date: January 17, 2010
  • Revised Date: June 02, 2010
  • A method for the determination of common organochlorine pesticides (OCPs) and polychlorinated biphenyls (PCBs) in groundwater by gas chromatography (GC) was developed. The method provides the detection limits of lower than 2.21 ng/L for OCPs, 5.20 ng/L for PCB 1 and lower than 1.30 ng/L for other target pollutants. The recoveries for most of the OCPs and PCBs were 63.5%~110.2% with precision of 2.2%~17.3% RSD (n=5) and the recoveries of the pollutants in practical samples were 87.34%~133.76% except for endrin. The method provides the advantages of good stability and reproducibility, simple sample preparation and has been applied to the determination of OCPs and PCBs in groundwater samples.
  • 孟阳,薛建良,刘广民,刘永健,李金春子.持久性有机污染物的环境分布与生物危害[J].污染防治技术,2008,21(6):68-72.
    陈威,王金波,孟庆庆.浅谈持久性有机物的特性、危害及对策[J].环境科学与管理,2009,34(7):37-38.
    EPA Method 8081B,Oraganochlorine pesticides by gas chromatography[S].

    EPA Method 8081B,Oraganochlorine pesticides by gas chromatography[S].
    EPA Method 8082A,Polychlorinated biphenyls by gas chromatography[S].

    EPA Method 8082A,Polychlorinated biphenyls by gas chromatography[S].
    甘平胜,黄聪,于鸿,李晓晶.毛细管柱气相色谱法测定饮用水中17种卤代有机物[J].中国卫生检验杂志,2009,19(5):1027-1028.
    曲仪,李树石,何英男.气相色谱法测定城市自来水中有机氯农药的残留[J]. 环境科学保护,2005,31(127):47-49.
    江锐曙,王丙涛.凉茶中有机氯农药残留的气相色谱检测方法研究[J].中国卫生检验杂志,2009,19(7):1463-1465.
    周双林,薛辉利,张晓辉,黄福勇.养殖水体中多氯联苯残留的气相色谱分析[J].福建分析测试,2009,18(3):55-57.
    唐彦君,郑树生,卢秀萍,王桂华,谷景霞.毛细柱气相色谱法快速测定大米中有机氯农药残留[J].黑龙江八一农垦大学学报,2006,18(1):63-66.
    安琼,董元华,倪俊,王辉,靳伟. 气相色谱法测定禽蛋中微量有机氯农药及多氯联苯残留[J].色谱,2002,20(2):167-171.
    张桃英,饶竹.快速溶剂萃取/气相色谱测定果蔬中有机氯农药残留的研究[J].农药科学与管理,2005,26(10):10-13.
    刘文长,陶文靖,程丽娅,余兴,田旻,黄琴,李胜生.超声提取-固相萃取小柱净化-气相色谱法测定土壤中14种有机氯农药[J].岩矿测试,2009,28(6):541-544.
    王玉,刘菲,孙玉梅,石峰.固相膜萃取富集大体积地下水中痕量半挥发有机污染物[J].理化检验:化学分册,2008,44(2):127-130.
    黄业茹,施钧慧,唐莉.GC/MS分析环境样品中的多氯联苯(PCBs)[J].分析测试技术与仪器,2000,6(4):216-224.
    Chen F,Chen L,Wang Q,Zhou J,Xue X,Zhao J. Determination of organochlorine pesticides in propolis by gas chromatography-electron capture detection using double column series solid-phase extraction[J]. Analytical and Bioanalytical Chemistry,2009,393:1073-1079.

    Chen F,Chen L,Wang Q,Zhou J,Xue X,Zhao J. Determination of organochlorine pesticides in propolis by gas chromatography-electron capture detection using double column series solid-phase extraction[J]. Analytical and Bioanalytical Chemistry,2009,393:1073-1079.
    Ozcan S, Tor A, Aydin M E. Application of ultra-sound-assisted emulsification-micro-extraction for the analysis of organochlorine pesticides in waters[J].Water Research,2009,43:4269-4277.

    Ozcan S, Tor A, Aydin M E. Application of ultra-sound-assisted emulsification-micro-extraction for the analysis of organochlorine pesticides in waters[J].Water Research,2009,43:4269-4277.
    Cortada C,Vidal L,Tejada S, Romo A, Canals A. Determination of organochlorine pesticides in complex matrices by single-drop microextraction coupled to gas chromatography-mass spectrometry[J].Analytica Chimica Acta,2009,638(1):29-35.

    Cortada C,Vidal L,Tejada S, Romo A, Canals A. Determination of organochlorine pesticides in complex matrices by single-drop microextraction coupled to gas chromatography-mass spectrometry[J].Analytica Chimica Acta,2009,638(1):29-35.
    Farahania H, Yaminia Y, Shariatib S, Khalili-Zanjania M R, Mansour-Baghahic S. Development of liquid phase microextraction method based on solidification of floated organic drop for extraction and preconcentration of organochlorine pesticides in water samples[J].Analytica Chimica Acta,2008,626(2):166-173.

    Farahania H, Yaminia Y, Shariatib S, Khalili-Zanjania M R, Mansour-Baghahic S. Development of liquid phase microextraction method based on solidification of floated organic drop for extraction and preconcentration of organochlorine pesticides in water samples[J].Analytica Chimica Acta,2008,626(2):166-173.
    唐卫红,夏凡,刘鸣.双柱双ECD检测器气象色谱仪测定有机氯农药方法的研究[J].上海环境科学,2004,23(4):168-172.

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