• Core Journal of China
  • DOAJ
  • Scopus
  • Chinese Scientific and Technical Papers and Citations (CSTPC)
  • Chinese Science Citation Database (CSCD)
Rapid Determination of SiO2,Al2O3,Fe2O3,TiO2,CaO and MgO in Magnesium-based Refractory Materials by X-ray Fluorescence Spectrometry with Powder Pellet Sample Preparation[J]. Rock and Mineral Analysis, 2008, 27(3): 232-234.
Citation: Rapid Determination of SiO2,Al2O3,Fe2O3,TiO2,CaO and MgO in Magnesium-based Refractory Materials by X-ray Fluorescence Spectrometry with Powder Pellet Sample Preparation[J]. Rock and Mineral Analysis, 2008, 27(3): 232-234.

Rapid Determination of SiO2,Al2O3,Fe2O3,TiO2,CaO and MgO in Magnesium-based Refractory Materials by X-ray Fluorescence Spectrometry with Powder Pellet Sample Preparation

More Information
  • Revised Date: October 08, 2007
  • A method for the determination of SiO2, Al2O3, Fe2O3, TiO2, CaO and MgO in magnesiumbased refractory materials by X-ay fluorescence spectrometry with powder pellet sample preparation was developed. The instrument operating parameters were optimized and a series of standard reference materials were used for the calibration. The matrix effect was corrected by using empirical coefficient method. The analytical precision of the method for major and minor components were less than 5% RSD(n=10). The method has been applied to the determination of these six components in magnesiumbased refractory materials with satisfactory results.
  • Related Articles

    [1]LI Yuan, DUAN Xiaoyan, SHI Yuge, LI Gang. Determination of Petroleum Oil in Soil by Fluorescence Spectrophotometry with Oscillatory Extraction[J]. Rock and Mineral Analysis, 2023, 42(6): 1240-1247. DOI: 10.15898/j.ykcs.202211150218
    [2]Xue-feng WANG, Chun-xue XU, Xue GU, Ya-ping WANG, Kai LI, Zheng-yu BAO. Concentration and Fractionation of Rare Earth Elements in Soils Surrounding Rare Earth Ore Area[J]. Rock and Mineral Analysis, 2019, 38(2): 137-146. DOI: 10.15898/j.cnki.11-2131/td.201807180085
    [3]HU De-xin, MA De-qi, AN Peng-sheng, WANG Zhen-kun, WANG Hong, LI Quan-bin, GU Song-hai, WEI Hong-bing. Determination of Water Soluble Fluoride, Chloride, Bromide and Nitrate in Iron Ores by Supersonic Extraction-Ion Chromatography[J]. Rock and Mineral Analysis, 2012, 31(2): 287-290.
    [4]XIAO Fang, TANG Zhi-yong, HAO Zhi-hong, SHUAI Qin, ZHENG Hong-tao, QIU Hai-ou. Determination of As(Ⅲ) and As(Ⅴ) in Stream Sediments by Hydride Generation-Atomic Fluorescence Spectrometry with Ultrasonic Extraction[J]. Rock and Mineral Analysis, 2011, 30(5): 545-549.
    [5]LIU Wenzhang, TAO Wenjing, CHENG Liya, YU Xing, TIAN Min, HUANG Qin, LI Shengsheng. Determination of Organochlorine Pesticides in Soil Samples by Gas Chromatography with Ultrasonic Extraction and Solid Phase Extraction[J]. Rock and Mineral Analysis, 2009, 28(6): 541-544.
    [6]Determination of 10 Elements including Silicon, Iron and Aluminum in Rock, Stream Sediment and Soil Samples by ICP-AES with Lithium Metaborate Fusion and Ultrasonic Extraction[J]. Rock and Mineral Analysis, 2008, 27(4): 287-290.
    [7]Speciation Analysis of Arsenic in Soil Samples[J]. Rock and Mineral Analysis, 2008, 27(3): 179-183.
    [8]Pre-treatment Methods for Analysis of Persistent Organic Pollutants in Soil Samples[J]. Rock and Mineral Analysis, 2008, 27(2): 81-86.
    [9]Comparison of Ultrasonic Vibration and Mechanical Shaking Extraction of Loosely Sorbed Phosphorus in Sediments[J]. Rock and Mineral Analysis, 2005, (3): 193-196.
    [10]Determination of BHC and DDT in Soil Samples by Ultrasonic Extraction and Gas Chromatography[J]. Rock and Mineral Analysis, 2003, (4): 248-253.

Catalog

    Article views (1624) PDF downloads (1196) Cited by()

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return