• Core Journal of China
  • DOAJ
  • Scopus
  • Chinese Scientific and Technical Papers and Citations (CSTPC)
  • Chinese Science Citation Database (CSCD)
Zhen-hua GUO, Han-jiang HE, Feng-ying TIAN. Determination of Rare Earth Elements in Phosphate Ores by Inductively Coupled Plasma-Mass Spectrometry with Mixed Acid Dissolution[J]. Rock and Mineral Analysis, 2014, 33(1): 25-28.
Citation: Zhen-hua GUO, Han-jiang HE, Feng-ying TIAN. Determination of Rare Earth Elements in Phosphate Ores by Inductively Coupled Plasma-Mass Spectrometry with Mixed Acid Dissolution[J]. Rock and Mineral Analysis, 2014, 33(1): 25-28.

Determination of Rare Earth Elements in Phosphate Ores by Inductively Coupled Plasma-Mass Spectrometry with Mixed Acid Dissolution

More Information
  • Received Date: March 10, 2013
  • Accepted Date: April 10, 2013
  • Published Date: December 31, 2013
  • It is known that a large amount of rare earth elements (REEs) is contained in phosphate rock, making it an important reserve of REEs after ion-type REEs ores. Therefore, it is significant to analyze and study the determination method for REEs in phosphate rock. Phosphate ore samples were digested with HF-HNO3-HCl-H2SO4-aqua regia. A method for the determination of 15 REEs in phosphate ores by Inductively Coupled Plasma-Mass Spectrometry (ICP-MS) was established. Some parameters affecting the determination, such as sample weight, sample digestion method, selected determination isotopes and interference correction were investigated. Matrix effect and sensitivity drift were monitored and corrected by an interior isotope of 103Rh. The recoveries of the method are 95.7%-108.0%, detection limits are 0.001-0.021 μg/g and precision (RSD) is less than 6% (n=12). The method is suitable for analysis of rare earth elements in phosphate ores.
  • Related Articles

    [1]CHEN Kai, LIU Fei, YANG Zihan, XIANG Xin. Review on the Determination of Oxidant Demand for in-situ Chemical Oxidation Application[J]. Rock and Mineral Analysis, 2023, 42(2): 271-281. DOI: 10.15898/j.cnki.11-2131/td.202202170023
    [2]ZHANG Xiaorui, WU Bailin, LEI Angui, YANG Songlin, YAO Luhang, PANG Kang, BAO Zhian, WANG Miao, HAO Xin, LIU Mingyi, LI Qi, LIN Zhouyang. In-situ Micro-scale Pb Isotope Identification Characteristics of Metallogenic and Non-metallogenic Pyrites in Sandstone-type Uranium Deposits[J]. Rock and Mineral Analysis, 2022, 41(5): 717-732. DOI: 10.15898/j.cnki.11-2131/td.202111300192
    [3]XIAO Zhi-bin, GENG Jian-zhen, TU Jia-run, ZHANG Ran, YE Li-juan, BI Jun-hui, ZHOU Hong-ying. In situ U-Pb Isotope Dating Techniques for Sandstone-type Uranium Deposits[J]. Rock and Mineral Analysis, 2020, 39(2): 262-273. DOI: 10.15898/j.cnki.11-2131/td.201908120129
    [4]Wei-meng ZHANG, Jie YAN, Fu-jun ZHONG, Jia-yong PAN, Wen-quan LIU, Jing LAI, Tang-bo ZHOU. In situ LA-ICP-MS U-Pb Dating of Uraninite from the Shijiaowei Granite-type Uranium Deposit, Northern Guangdong Province[J]. Rock and Mineral Analysis, 2019, 38(4): 449-460. DOI: 10.15898/j.cnki.11-2131/td.201901160007
    [5]Miao TIAN, Qing-guo MENG, Chang-ling LIU, Cheng-feng LI, Gao-wei HU, Juan FENG, Quan-sheng ZHAO. Parameter Optimization and Analysis Method for Determination of Natural Gas Hydrate by Powder X-ray Diffraction[J]. Rock and Mineral Analysis, 2017, 36(5): 481-488. DOI: 10.15898/j.cnki.11-2131/td.201703160033
    [6]Shan-ling FU, Cheng-hai ZHAO. Progress of in situ U-Th/He Isotopic Dating Technique and Its Application to Low Temperature Deposits[J]. Rock and Mineral Analysis, 2017, 36(1): 1-13. DOI: 10.15898/j.cnki.11-2131/td.2017.01.002
    [7]Zhi-xiong LI, Yi-tong HAN, Yong-qiang XU, Yang YANG, Jia-wei CHEN. In Situ Measurement of Aggregation Effect of Nanoscale Zero-valent Iron in the Presence of Natural Organic Matter Based on the Dynamic Light Scattering Technique[J]. Rock and Mineral Analysis, 2016, 35(6): 634-641. DOI: 10.15898/j.cnki.11-2131/td.2016.06.010
    [8]Sheng-xuan HUANG, Xiang WU, Shan QIN. Research Progress on in situ Experimental and Theoretical Simulations of Element Partitioning under High Temperature and High Pressure[J]. Rock and Mineral Analysis, 2016, 35(2): 117-126. DOI: 10.15898/j.cnki.11-2131/td.2016.02.002
    [9]Jiao-hua ZHOU, Jian-yu WANG, Ming-xin GU, Zhen WANG. The Main Mineral Typomorphic Characteristics of the Henan Tangjiaping Molybdenum District Using X-ray Diffraction and Rock Mineral Identification Technology[J]. Rock and Mineral Analysis, 2015, 34(1): 82-90. DOI: 10.15898/j.cnki.11-2131/td.2015.01.011
    [10]Development of a Portable Extinction Photometer and Its Application to in situ Rapid Detection of Adulterated Milk[J]. Rock and Mineral Analysis, 2008, 27(3): 169-173.

Catalog

    Article views (3056) PDF downloads (38) Cited by()

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return