Citation: | QIAO Songfen,QIN Chong,LIU Aiqin,et al. Determination of Three Nitrophenol Compounds in Soil by Ultrasonic Extraction-High Performance Liquid Chromatography-Mass Spectrometry[J]. Rock and Mineral Analysis,2024,43(3):501−508. DOI: 10.15898/j.ykcs.202303170036 |
As important organic chemical raw materials, nitrophenol compounds have high toxicity and carcinogenicity, which can be transmitted into soil through air and water, causing pollution and endangering human health. In the past, nitrophenol compounds in soil were usually determined by gas chromatography and gas chromatography-mass spectrometry. The derivatization was usually required to improve the sensitivity, which was time-consuming and cumbersome. To achieve a rapid and accurate analysis of the three nitrophenol compounds in soil, a method of ultrasonic extraction-high performance liquid chromatography-mass spectrometry (HPLC-MS) was established. The nitrophenol compounds in soil were extracted by ultrasonic extraction with dichloromethane/