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天然水体中汞形态分析

陈娟, 余晓平, 郭亚飞, 邓天龙

陈娟, 余晓平, 郭亚飞, 邓天龙. 天然水体中汞形态分析[J]. 岩矿测试, 2012, 31(6): 939-944.
引用本文: 陈娟, 余晓平, 郭亚飞, 邓天龙. 天然水体中汞形态分析[J]. 岩矿测试, 2012, 31(6): 939-944.
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CHEN Juan, YU Xiao-ping, GUO Ya-fei, DENG Tian-long. Speciation Analysis of Mercury in Natural Water[J]. Rock and Mineral Analysis, 2012, 31(6): 939-944.
Citation: CHEN Juan, YU Xiao-ping, GUO Ya-fei, DENG Tian-long. Speciation Analysis of Mercury in Natural Water[J]. Rock and Mineral Analysis, 2012, 31(6): 939-944.
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天然水体中汞形态分析

  • 1.

    天津科技大学, 天津市海洋资源与化学重点实验室, 天津 300457

  • 2.

    成都理工大学材料与化学化工学院, 四川 成都 610059

  • 3.

    天津科技大学, 天津市海洋资源与化学重点实验室, 天津 300457

  • 4.

    中国科学院青海盐湖研究所, 盐湖资源与化学重点实验室, 青海 西宁 810008

  • 5.

    天津科技大学, 天津市海洋资源与化学重点实验室, 天津 300457

  • 6.

    成都理工大学材料与化学化工学院, 四川 成都 610059

  • 7.

    天津科技大学, 天津市海洋资源与化学重点实验室, 天津 300457

  • 8.

    成都理工大学材料与化学化工学院, 四川 成都 610059

  • 9.

    中国科学院青海盐湖研究所, 盐湖资源与化学重点实验室, 青海 西宁 810008

基金项目: 

教育部博士学科点科研专项(20101208110003)

天津市科技支撑重点项目(11ZCKFGX2800)

国家自然科学基金重点项目(2083600)

天津市特聘教授人才引进启动基金(20100405)

Speciation Analysis of Mercury in Natural Water

  • 1.

    Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China

  • 2.

    College of Materials, Chemistry and Chemical Engineering, Chengdu University of Technology, Chengdu 610059, China

  • 3.

    Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China

  • 4.

    Key Laboratory of Salt Lakes Resources and Chemistry, Chinese Academy of Sciences, Qinghai Institute of Salt Lakes, Xining 810008, China

  • 5.

    Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China

  • 6.

    College of Materials, Chemistry and Chemical Engineering, Chengdu University of Technology, Chengdu 610059, China

  • 7.

    Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China

  • 8.

    College of Materials, Chemistry and Chemical Engineering, Chengdu University of Technology, Chengdu 610059, China

  • 9.

    Key Laboratory of Salt Lakes Resources and Chemistry, Chinese Academy of Sciences, Qinghai Institute of Salt Lakes, Xining 810008, China

摘要

    摘要
  • 摘要: 简要归纳了天然水体中汞形态分析的分离(萃取、吸附、电化学分离、色谱)及检测技术(分光光度法、原子光谱法、质谱法、电化学分析法),指出了未来针对痕量超痕量汞形态分析新技术主要集中在样品前处理和便携式在线现场分析,着重推荐高效、经济并具有广阔应用前景的液相色谱-氢化物发生原子荧光光谱(LC-HG-AFS)用于痕量超痕量汞形态分析。
    Abstract: Separation techniques (extraction, adsorption, electrochemical separation and chromatography) and detection techniques (Spectrophotometry, Atomic Spectrometry, Mass Spectrometry and Electrochemical Analysis) for mercury species in natural water are briefly reviewed in this paper from 22 references. New approaches for trace and ultra-trace mercury speciation analysis in the future should focus on pretreatment system or exploiting a portable instrument so as to realize the species analysis in situ. Moreover, it is worthy mentioning that Liquid Chromatography-Hydrate Generation-Atomic Fluorescence Spectrometry (LC-HG-AFS) with low cost and good performance will have a bright prospect for trace and ultra trace mercury species analysis.
    • HTML全文
    • 参考文献(21)
  • Yin Y G, Chen M, Peng J F, Liu J F, Jing G B. Dithizone-functionalized solid phase extraction-displacement elution-high performance liquid chromatography-inductively coupled plasma mass spectrometry for mercury speciation in water samples [J]. Talanta, 2010, 81: 1788-1792.

    Yin Y G, Chen M, Peng J F, Liu J F, Jing G B. Dithizone-functionalized solid phase extraction-displacement elution-high performance liquid chromatography-inductively coupled plasma mass spectrometry for mercury speciation in water samples [J]. Talanta, 2010, 81: 1788-1792.
    Segade S R, Tyson J F. Determination of methylmercury and inorganic mercury in water samples slurry sampling cold vapor atomic absorption spectrometry in a flow injection system after preconcentration on silica C18 modifed [J]. Talanta,2007, 71: 1696-1702.

    Segade S R, Tyson J F. Determination of methylmercury and inorganic mercury in water samples slurry sampling cold vapor atomic absorption spectrometry in a flow injection system after preconcentration on silica C18 modifed [J]. Talanta,2007, 71: 1696-1702.
    Margetinov J, Houserova-Pelcova P, Kuban V. Speciation analysis of mercury in sediments, zoobenthos and river water samples by high-performance liquid chromatography hyphenated to atomic fluorescence spectrometry following preconcentration by solid phase extraction [J]. Analytica Chimica Acta, 2008, 615: 115-123.

    Margetinov J, Houserova-Pelcova P, Kuban V. Speciation analysis of mercury in sediments, zoobenthos and river water samples by high-performance liquid chromatography hyphenated to atomic fluorescence spectrometry following preconcentration by solid phase extraction [J]. Analytica Chimica Acta, 2008, 615: 115-123.
    Falter R, Schöler H E. Determination of mercury species in natural waters at picogram level with on-line RP C18 preconcentration and HPLC-UV-PCO-CVAAS [J]. Fresenius' Journal of Analytical Chemistry,1995, 353: 34-38.

    Falter R, Schöler H E. Determination of mercury species in natural waters at picogram level with on-line RP C18 preconcentration and HPLC-UV-PCO-CVAAS [J]. Fresenius' Journal of Analytical Chemistry,1995, 353: 34-38.
    Demuth N, Heumann K G. Validation of methylmercury detection methods for GC analysis using ICP-MS [J]. Analytical Chemistry, 2001, 73: 4020-4027.

    Demuth N, Heumann K G. Validation of methylmercury detection methods for GC analysis using ICP-MS [J]. Analytical Chemistry, 2001, 73: 4020-4027.
    Sanz J, Diego A, Raposo J C, Madariaga J M. Routine analysis of mercury species using commercially available instrumentation: Chemometric optimisation of the instrumental variables [J]. Analytica Chimica Acta,2003, 486: 255-267.

    Sanz J, Diego A, Raposo J C, Madariaga J M. Routine analysis of mercury species using commercially available instrumentation: Chemometric optimisation of the instrumental variables [J]. Analytica Chimica Acta,2003, 486: 255-267.
    Santos J S, Guárdia M, Augustin P, Santosam L P. Determination of organic and inorganic mercury species in water and sediment samples by HPLC on-line coupled with ICP-MS [J]. Talanta, 2009, 80: 207-211.

    Santos J S, Guárdia M, Augustin P, Santosam L P. Determination of organic and inorganic mercury species in water and sediment samples by HPLC on-line coupled with ICP-MS [J]. Talanta, 2009, 80: 207-211.
    Chen H, Chena J, Jina X Z, Wei D. Determination of trace mercury species by high performance liquid chromatography-inductively coupled plasma mass spectrometry after cloud point extraction [J]. Journal of Hazardous Materials, 2009, 172: 1282-1287.

    Chen H, Chena J, Jina X Z, Wei D. Determination of trace mercury species by high performance liquid chromatography-inductively coupled plasma mass spectrometry after cloud point extraction [J]. Journal of Hazardous Materials, 2009, 172: 1282-1287.
    Stalikas C D. Micelle-mediated extraction as a tool for separation and preconcentration in metal analysis [J]. TrAC Trends in Analytical Chemistry, 2002, 21: 343-355.

    Stalikas C D. Micelle-mediated extraction as a tool for separation and preconcentration in metal analysis [J]. TrAC Trends in Analytical Chemistry, 2002, 21: 343-355.
    Carrasco L, Díez S, Bayona J M. Simultaneous deter- mination of methyl- and ethyl-mercury by solid-phase microextraction followed by gas chromatography atomic fluorescence detection [J]. Journal of Chromatography A, 2009, 1216: 8828-8834.

    Carrasco L, Díez S, Bayona J M. Simultaneous deter- mination of methyl- and ethyl-mercury by solid-phase microextraction followed by gas chromatography atomic fluorescence detection [J]. Journal of Chromatography A, 2009, 1216: 8828-8834.
    Zierhut A, Leopold K, Harwardt L, Worsfold P, Schustr M. Activated gold surfaces for the direct preconcentration of mercury species from natural waters [J]. Journal of Analytical Atomic Spectrometry, 2009, 24: 767-774.

    Zierhut A, Leopold K, Harwardt L, Worsfold P, Schustr M. Activated gold surfaces for the direct preconcentration of mercury species from natural waters [J]. Journal of Analytical Atomic Spectrometry, 2009, 24: 767-774.
    Zierhut A, Leopold K, Harwardt L, Schuster M. Analysis of total dissolved mercury in waters after on-line preconcentration on an active gold column [J]. Talanta, 2010, 81: 1529-1535.

    Zierhut A, Leopold K, Harwardt L, Schuster M. Analysis of total dissolved mercury in waters after on-line preconcentration on an active gold column [J]. Talanta, 2010, 81: 1529-1535.
    Hong L R. Speciation of mercury by capillary clectro-phoresis [J]. Guangdong Trace Elements Science, 2006, 33: 43-45.

    Hong L R. Speciation of mercury by capillary clectro-phoresis [J]. Guangdong Trace Elements Science, 2006, 33: 43-45.
    Carrasco L, Dｉez S, Bayona J M. Methylmercury deter-mination in biota by solid-phase microextraction matrix effect evaluation [J]. Journal of Chromatography A, 2007, 1174: 2-6.

    Carrasco L, Dｉez S, Bayona J M. Methylmercury deter-mination in biota by solid-phase microextraction matrix effect evaluation [J]. Journal of Chromatography A, 2007, 1174: 2-6.
    Chen K, Hsu I, Sun Y. Determination of methylmercury and inorganic mercury by couplingshort-column ion chromatographic separation, on-line photocatalyst-assisted vapor generation, and inductively coupled plasma mass spectrometry [J]. Journal of Chromatography A, 2009, 1216: 8933-8938.

    Chen K, Hsu I, Sun Y. Determination of methylmercury and inorganic mercury by couplingshort-column ion chromatographic separation, on-line photocatalyst-assisted vapor generation, and inductively coupled plasma mass spectrometry [J]. Journal of Chromatography A, 2009, 1216: 8933-8938.
    Gómez-Ariza J L, Lorenzo F, García-Barrera T. Compa-rative study of atomic fluorescence spectroscopy and inductively coupled plasma mass spectrometry for mercury and arsenic multispeciation [J]. Analytical and Bioanalytical Chemistry, 2005, 382: 485-492.

    Gómez-Ariza J L, Lorenzo F, García-Barrera T. Compa-rative study of atomic fluorescence spectroscopy and inductively coupled plasma mass spectrometry for mercury and arsenic multispeciation [J]. Analytical and Bioanalytical Chemistry, 2005, 382: 485-492.
    Moghaddam H H, Tehrani M S. Sensitive mercury speciation by reversed-phase column high-performance liquid chromatography with UV-visible detection after solid-phase extraction using 6-mercaptopurine and dithizone [J]. Journal of AOAC International, 2008, 91: 1453-1458.

    Moghaddam H H, Tehrani M S. Sensitive mercury speciation by reversed-phase column high-performance liquid chromatography with UV-visible detection after solid-phase extraction using 6-mercaptopurine and dithizone [J]. Journal of AOAC International, 2008, 91: 1453-1458.
    Wurl O, Elsholz O, Ebinghaus R. Flow system device for the on-line determination of total mercury in seawater [J]. Talanta, 2000,52: 51-57.

    Wurl O, Elsholz O, Ebinghaus R. Flow system device for the on-line determination of total mercury in seawater [J]. Talanta, 2000,52: 51-57.
    Válega M, Abreu S, Pato P, Rocha L, Gome A R, Preeira M E, Duarte A C. Determination of organic mercury in biota, plants and contaminated sediments using a thermal atomic absorption spectrometry technique [J]. Water, Air, and Soil Pollution, 2006, 174: 223-234.

    Válega M, Abreu S, Pato P, Rocha L, Gome A R, Preeira M E, Duarte A C. Determination of organic mercury in biota, plants and contaminated sediments using a thermal atomic absorption spectrometry technique [J]. Water, Air, and Soil Pollution, 2006, 174: 223-234.
    Rodil R, Carro A M, Lorenzo R A, Abuｉn M, Cela R.Methylmercury determination in biological samples by derivatization, solid-phase microextraction and gas chromatography with microwave-induced plasma atomic emission spectrometry [J].Journal of Chromatography A, 2002, 963: 313-323.

    Rodil R, Carro A M, Lorenzo R A, Abuｉn M, Cela R.Methylmercury determination in biological samples by derivatization, solid-phase microextraction and gas chromatography with microwave-induced plasma atomic emission spectrometry [J].Journal of Chromatography A, 2002, 963: 313-323.
    Canário J, Antunes P, Lavrado J, Vale C. Simple method for monomethylmercury determination in estuarine sediments [J]. TrAC Trends in Analytical Chemistry, 2004, 23: 799-805.

    Canário J, Antunes P, Lavrado J, Vale C. Simple method for monomethylmercury determination in estuarine sediments [J]. TrAC Trends in Analytical Chemistry, 2004, 23: 799-805.
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出版历程
  • 收稿日期:  2011-10-31
  • 修回日期:  2012-04-19
  • 发布日期:  2012-11-09

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