碳酸钙共沉淀-火焰原子吸收光谱法测定卤水中痕量铜铅锌
Determination of Trace Copper, Lead and Zinc in Brines by FAAS after Co-precipitation with Calcium Carbonate
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摘要: 以碳酸钙共沉淀卤水中的痕量Cu、Pb、Zn,用火焰原子吸收光谱法测定。对试剂的加入量、富集时间、酸度等影响因素进行了实验,选择了最佳的共沉淀条件。方法已用于卤水分析,加标回收率为Cu94.0%~97.6%、Pb94.0%。102%、Zn93.4%-102%。对卤水样品6次测定的相对标准偏差为Cu0.49%、Pb0.79%、Zn1.85%。Abstract: Trace copper,lead and zinc in brines were determined by flame atomic absorption spectrometry after separation and pre-concentration by co-precipitation with calcium carbonate.Some parameters influencing the co-precipitation separation,including(amounts) o