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LI Pei-chang, HAN Bin, ZHANG Peng, CAO Lei, ZHENG Xiao-ling, HE Ying, WANG Xiao-ru. Gas Chromatographic Analysis of the Fatty Acid Components in Soil Samples[J]. Rock and Mineral Analysis, 2010, 29(4): 363-367.
Citation: LI Pei-chang, HAN Bin, ZHANG Peng, CAO Lei, ZHENG Xiao-ling, HE Ying, WANG Xiao-ru. Gas Chromatographic Analysis of the Fatty Acid Components in Soil Samples[J]. Rock and Mineral Analysis, 2010, 29(4): 363-367.
shu

Gas Chromatographic Analysis of the Fatty Acid Components in Soil Samples

  • 1.

    First Institute of Oceanography State Oceanic Administration, Qingdao 266061, China

  • 2.

    First Institute of Oceanography State Oceanic Administration, Qingdao 266061, China

  • 3.

    Huantai Environment Protection Bureau, Zibo 256400, China

  • 4.

    First Institute of Oceanography State Oceanic Administration, Qingdao 266061, China

  • 5.

    Shanghai Ocean University, Shanghai 201306, China

  • 6.

    First Institute of Oceanography State Oceanic Administration, Qingdao 266061, China

  • 7.

    First Institute of Oceanography State Oceanic Administration, Qingdao 266061, China

  • 8.

    First Institute of Oceanography State Oceanic Administration, Qingdao 266061, China

More Information
  • Received Date: November 09, 2009
  • Revised Date: March 21, 2010
    Abstract
  • A method for the determination of components in fatty acid in soil samples was established. Fatty acid components in the samples were separated and identified by gas chromatography-mass spectrometry (GC-MS) and each component was quantified by GC with standard solution calibration. The linear correlation coefficients (R2) of the method for each component were 0.9913~0.9999. The detection limits of the method for the components were 0.016~0.038 mg/L. Average recovery of the method was 97.86% with precision of 0.73%~2.57%RSD(n=6). The method has been applied to the quantitative analysis of fatty acid components in soil samples with satisfactory results.
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  • 于树,汪景宽,李双异.应用PLFA方法分析长期不同施肥处理对玉米地土壤微生物群落结构的影响[J].生态学报,2008,28(9):4221-4227.
    白震,何洪波,张威,解宏图,张旭东,王鸽.磷脂脂肪酸技术及其在土壤微生物研究中的应用[J].生态学报,2006,26(7):2388-2394.
    王曙光,侯彦林.磷脂脂肪酸方法在土壤微生物分析中的应用[J].微生物学通报,2004,31(1):114-117.
    蔡燕飞,廖宗文.FAME法分析施肥对番茄青枯病抑制和土壤健康恢复的效果[J].中国农业科学,2003,36(8):922-927.
    颜备战,胡凯,贾蓉芬.脂肪酸在古土壤和黄土层的分布差异及其环境指示意义[J].江苏地质,1996,20(4):237-241.
    林九皓,谌丽蓉.土壤脂肪酸的油、气化学勘探研究[J].矿物学报,1995,15(1):21-28.
    雷黎立,常国斌,王克华,王存波,陈国宏.安卡鸡肌肉脂肪酸组分的气相色谱-质谱联合分析[J].安徽农业科学,2009,37(13):5819-5820.
    侯冬岩,回瑞华,李铁纯,邢晓燕,刘晓媛,刁全平.稻谷副产品中脂肪酸的气相色谱-质谱分析[J].分析试验室,2009,28(5): 61-63.
    孙伟红,冷凯良,王志杰,宁劲松,王瑜,刘艳萍,翟毓秀.浒苔的氨基酸和脂肪酸组成研究[J].渔业科学进展,2009,30(2):106-109.
    张治远,赵燕,杨兴斌,吕游.气相色谱-质谱法分析牛至中挥发油与脂肪酸成分[J].医学导报,2009,28(5):549-552.
    彭书明,梁山,何建,雷泞菲,潘丽娟,温爱丹.瓜蒌籽中脂肪酸的气相色谱分析[J].时珍国医国药,2009,20(5):1197-1198.
    刘文长,陶文靖,程丽娅,余兴,田旻,黄勤,李胜生.超声提取-固相萃取小柱净化-气相色谱法测定土壤中14种有机氯农药[J].岩矿测试,2009,28(6):541-544.
    傅伟昌,陈尚卫,顾小红,汤坚,蒋再良.癞葡萄籽油的脂肪酸分布分析及共轭亚麻酸的鉴定[J].中国油脂,2009,34(5):75-79.
    徐静,陆建平.气相色谱法测定茶叶中的脂肪酸组成[J].化工技术与开发,2009,38(4):39-41.
    祝洪艳,张琪,夏从立,孟祥颖,鲍永利,于春雷,乌垠,李玉新.千金子油理化性质及其脂肪酸和挥发油成分分析[J].分子科学学报,2009,25(2):90-94.
    张永辉,阎萍,梁春年,曾玉峰.青海大通牦牛肌间脂肪酸组成分析[J].农业科技,2009,10(1):148.
    徐竞.兔肉脂肪酸组成的气相色谱法分析[J].肉类工业,2009,336(4):31-32.
    张纵圆,李茂华,张涛.新疆紫花苜蓿籽脂肪酸化学成分的分析[J].光谱实验室,2009,26(2):354-356.
    张述琼,孙毅毅,赵燕.亚麻种子油提取工艺及脂肪酸组成的GC-MS分析[J].药学服务与研究,2009,9(2):134-136.
    侯雪丹,吴培,张毅,许喜林.有机溶剂耐受性酵母细胞的脂肪酸组成分析[J].现代食品科技,2009,25(5):573-576.
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